J. Wrba scite author profile

A red‐brown zirconium nitride was prepared by ammonolysis of ZrCl4. Chemical analysis leads to a composition of Zr3N4. It is not possible to distinguish between the space groups Pnam and Pna21 in the case of Zr3N4 using powder methods. The lattice constants are: a = 972.94(5) pm, b = 1081.75(6) pm, c = 328.10(1) pm (Z = 4). X‐ray powder diffraction data were used for structure refinement. The high temperature behavior was investigated with in situ XRD methods. Zr3N4 decomposes into ZrN and nitrogen gas at temperatures above 800°C.

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Recent developments of Mn–Zn ferrites for high permeability applications

Ott¹,

Wrba²,

Lucke³

2003

Journal of Magnetism and Magnetic Materials

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Synthesis and Characterization of Oxynitrides in the ZrO2-Rich Part of the Systems Ca–Zr–O–N and Mg–Zr–O–N

Lerch

Hock

et al. 1997

Journal of Solid State Chemistry

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Formation of rock salt-type Zr(N,O,C) phases by carbothermal nitridation of zirconia

Lerch

Wrba

1996

J Mater Sci Lett

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Phase relationships in the ZrO2-rich part of the systems Y-Zr-N-O, Ca-Zr-N-O, and Mg-Zr-N-O up to temperatures of 1150 °C

Wrba

Lerch

1998

Journal of the European Ceramic Society

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J. Wrba

Synthesis, Crystal Structure, and High Temperature Behavior of Zr₃N₄

Recent developments of Mn–Zn ferrites for high permeability applications

Synthesis and Characterization of Oxynitrides in the ZrO2-Rich Part of the Systems Ca–Zr–O–N and Mg–Zr–O–N

Formation of rock salt-type Zr(N,O,C) phases by carbothermal nitridation of zirconia

Phase relationships in the ZrO2-rich part of the systems Y-Zr-N-O, Ca-Zr-N-O, and Mg-Zr-N-O up to temperatures of 1150 °C

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J. Wrba

Synthesis, Crystal Structure, and High Temperature Behavior of Zr3N4

Recent developments of Mn–Zn ferrites for high permeability applications

Synthesis and Characterization of Oxynitrides in the ZrO2-Rich Part of the Systems Ca–Zr–O–N and Mg–Zr–O–N

Formation of rock salt-type Zr(N,O,C) phases by carbothermal nitridation of zirconia

Phase relationships in the ZrO2-rich part of the systems Y-Zr-N-O, Ca-Zr-N-O, and Mg-Zr-N-O up to temperatures of 1150 °C

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Product

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Synthesis, Crystal Structure, and High Temperature Behavior of Zr₃N₄