The purpose of this study was to fabricate and evaluate the morphological structure of microporous anodic oxidation (MAO) or nanoporous anodic oxidation (NAO) treated titanium-silver (Ti-Ag) alloys. The Ti-Ag alloys were arc melted, homogenized, and quenched in water at room temperature. The MAO treatment was performed using β-glycerol phosphate (β-GP) and calcium acetate (CA) solution; the NAO treatment was performed using hydrofluoric acid (

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In this study, the osteoconductive properties of novel cyanoacrylate-based filling materials for bone defect were evaluated. A new filling material was prepared by mixing Histoacryl® and acid-treated -tricalcium phosphate ( -TCP). Mixing weight ratio of acid-treated -TCP to Histoacryl® was 5:1. 12 male Spraque-Dawley rats were used in this study. The animals were divided into 4 groups. Critical-sized calvarial defects (8 mm) were created in 9 animals, and then the defects were treated with dense pellet specimen, porous cement-like specimen, and untreated defect for surgical control group. Augmentation treatments were carried out in 3 animals. Histological analysis revealed excellent ostgeoconductive properties of new filling materials. But, some of -TCP particle in the cement-like group were encapsulated by fibrous connective tissue. For the dense pellet group and augmentation treatment group, shape and stability were better maintained during the implantation time than cement like group. These results indicate that our novel -TCP/Histoacryl® composite have the potential to serve as filling materials for bone defects in the dental and plastic surgery.

The aim of this study was to develop Au-Pt-Pd-Si alloys with metal-resin bonding properties optimized for dental restorations. The amount of silicon added ranged from 0.00-0.54 wt.%. The Au-Pt-Pd-Si alloys were manufactured using an arc melting furnace. They were homogenized at 800°C in air and cold rolled to a 1 mm thickness. The changes in the surface morphology and oxide layer formation were analyzed using scanning electron microscopy, energy dispersive X-ray spectroscopy, electron probe microanalysis and X-ray photoelectron spectroscopy before and after oxidation treatment. The mechanical properties of the alloys were evaluated using micro-hardness and shear bonding tests. The surface oxide layer was mostly composed of silicon dioxide and metallic gold. The micro-hardness of the Au-Pt-Pd-Si alloys increased as a function of the silicon concentration. The shear bonding strength was significantly higher (9.30 MPa) at 0.54 wt.% silicon (p < 0.05).