Iron-based amorphous alloys have attracted technological and scientific interests due to their excellent soft magnetic properties. In the present study, Ni0.5Zn0.5Fe2O4/Fe76Si9B10P5 soft magnetic composites cylinder of 15 mm diameter and 3 mm thickness was prepared by spark plasma sintering at the temperature of 780 K. The amorphous Fe-based soft magnetic composites Ni0.5Zn0.5Fe2O4/Fe76Si9B10P5 exhibited good magnetic properties after annealing treatment at temperature ranging from 643 K to 743 K. The beneficial effects of treatment under different temperatures were discussed in terms of the improved magnetic performance of Ni0.5Zn0.5Fe2O4/Fe76Si9B10P5 soft magnetic composites.
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