Coagulating sedimentation and oxidation treatment of process water in iron ore flotation of Yuanjiacun iron mine had been studied. The process water of this mine carried residual polyacrylamide (PAM), poly(diallyldimethylammonium chloride) (PDADMAC), and Ca 2+ from the flotation and caused decrease of the iron flotation recovery or grade of the concentrate. The studies on highintensity magnetic separation (HIMS) tailings for coagulating sedimentation showed that the settling performance of coagulant (named CYH) was better than that of PDADMAC. The analyses of FTIR spectra and zeta potential demonstrated that CYH is adsorbed mainly through electrostatic attraction onto HIMS tailings. Sodium hypochlorite was adopted to oxidize the residual organics in tailings wastewater. When sodium hypochlorite is at the dosage of 1.0 g/L, reaction temperature is of 20 ∘ C, and reaction time is of 30 minutes, the removal rates of PAM, COD, and Ca 2+ were 90.48%, 83.97%, and 85.00%, respectively. Bench-scale flotation studies on the treated tailings wastewater indicated that the iron recovery and grade of concentrate were close to those of freshwater.
The flotation separation on chlorite and hematite with the new modified fatty acid collector CY-23 was studied. The investigation included both flotation and reagent adsorption tests. And all the characteristics of chlorite surface before and after the adsorption of new collector CY-23 have been studied with X-ray photoelectron spectroscopy (XPS). The flotation results showed that caustic starch (CS) could depress the flotation of hematite and chlorite and CaCl 2 could activate chlorite flotation but failed on hematite when using CY-23 as collector. The adsorption rate of CY-23 on the surface of chlorite after being inhibited by CS was relatively smaller, but the amount of CY-23 adsorbed on the inhibited chlorite was greatly increased after adding activator CaCl 2 . The results of XPS analysis showed that the photoelectron spectroscopy peaks of Mg2p and Al2p moved towards low energy after collector CY-23 was absorbed on chlorite surface, which indicated that chemical bonding through electron cloud transfer occurred between collector CY-23 and Mg, Al ions of chlorite surface. The chemical reaction promoted the adsorption of CY-23 on chlorite surface and eventually improved the ability of CY-23 to float and collect chlorite.
Through the study on technological mineralogy of anshan type lean hematite ore, proved the stope in the southern district of ore minerals in the ore is mainly hematite, limonite, magnetite, hematite, siderite images, accounts for some 40% of the content of rock,the gangue minerals are mainly quartz, orthoclase and actinolite, accounts for some 60% of the content of rock,.The central ore minerals in the ores mainly are hematite, martite, magnetite, siderite, accounts for about 42% of the content of rock, the gangue minerals are mainly quartz and chlorite. about 58% of rock content. Ore minerals in the ore mainly has illusion, hematite, magnetite and hematite siderite, accounts for about 40% of the content of rock. The gangue minerals are mainly quartz and chlorite, accounts for about 60% of the content of rocks. At the same time, find out the main chemical components, mineral composition of ore district, embedded features and disseminated extent change.
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