Supercritical CO2 was used as solvent for the extraction of aucubin from the seeds of Eucommia ulmoides Oliv. The co-solvent composition was tested and extraction conditions were optimized. Results showed that the best co-solvent was a waterethanol mixture (1 + 3, v/v), and the highest yield was obtained when the extraction was performed under 26 MPa at extraction and separation temperatures of 55 and 30C for 120 min, using 6 mL co-solvent/g material at a CO2 flow rate of 20 L/h. In a comparison of the supercritical CO2 and Soxhlet extraction methods, the Soxhlet method needed 3 h to extract 10 g material, whereas the supercritical CO2 extraction technique needed only 2 h to extract 100 g material, thus showing a high extraction capability. The supercritical CO2 extraction produced a higher yield, with a lower cost for the extraction. Owing to the advantages of low extraction temperature, high yield, and ease of separating the product from the solvent, supercritical CO2 extraction is likely to be developed into an ideal technique for the extraction of aucubin, a compound with thermal instability, from the seeds of this plant.

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Thermal protection is still one of the key challenges for successful scramjet operations. In this study, the three-dimensional coupled heat transfer between high-temperature gas and regenerative cooling panel with kerosene of supercritical pressure flowing in the cooling channels was numerically investigated to reveal the fundamental characteristics of regenerative cooling as well as its influencing factors. The SST k-ω turbulence model with low-Reynolds-number correction provided by the pressure-based solver of Fluent 19.2 is adopted for simulation. It was found that the heat flux of the gas heated surface is in the order of 106 W/m2, and it declines along the flow direction of gas due to the development of boundary layer. Compared with cocurrent flow, the temperature peak of the gas heated surface in counter flow is much higher. The temperature and heat flux of the gas heated surface both rises with the static pressure and total temperature of gas. The heat flux of the gas heated surface increases with the mass flow rate of kerosene, and it hardly changes with the pressure of kerosene. Results herein could help to understand the real heat transfer process of regenerative cooling and guide the design of thermal protection systems.

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