In the present study, glass foams made of ground soda-lime glass obtained from transparent glass bottles and dolomite were investigated. The objective of this paper was to evaluate the influence of the heating rate on the microstructure of the obtained material and on its properties. The technological characterization of the ceramic bodies involved the determination of the volumetric expansion and average diameter of the pore. The microstructure was investigated by optical microscopy and scanning electron microscopy. Experimental results showed that the heating rate influenced both the volumetric expansion and the average diameter of the pore. Lower heating rates resulted in lower volumetric expansions since more CO(2) escaped from within the ceramic body.

The purpose of this study was to evaluate the production feasibility of triaxial whiteware using sand from cast iron moulds as a raw material instead of silica, and recycled glass in place of feldspar. Formulations were prepared using sand, glass waste, and white-firing clay such that only 50% of the composition was virgin material (clay). The ceramic bodies were formed by pressing and fired at different temperatures (between 1100 and 1300 degrees C). Specimens were characterized in terms of green density prior to firing; and their flexural strength, linear shrinkage, and water absorption were measured after firing. The microstructure was determined by scanning electron microscopy. Possible environmental impacts of this recycling process were also evaluated, through solubility and leaching tests, according to Brazilian standards. Gaseous emissions during the firing process were also analysed. The results showed that it is possible to produce triaxial ceramics by using such alternative raw materials.

No abstract

In this work micrometric particles of WC and Co were processed by high energy ball milling in a planetary ball mill. We evaluated the phase formation and changes in microstructure of WC-12wt%Co as a result of the following milling parameters: ball-to-powder weight ratio, milling time and speed. The material was characterized by X-ray diffraction (crystalline phases and crystallite size), particle size analysis (average grain diameter), the BET method (surface area), and scanning electron microscopy (powder morphology). The average particle size (D50) and crystallite size were respectively 1.63µm and 13.8nm, for a surface area of 4.709 m 2 /g, using a ball-to-powder weight ratio of 1:20, a milling time of 5h and a milling speed of 500 rpm.

No abstract