Dewatering of Ionic Liquids in a Falling Film EvaporatorExperimental investigations on the dewatering of ionic liquids (IL) in a single falling film evaporator were carried out.Depending on the process conditions, such as heating temperature and process pressure, a minimum water content of 0.2 wt-% (2000 ppm) was achieved using batch mode. Assuming that these water contents represent equilibrium state at constant temperatures and pressures, vapor pressure curves of different IL-water mixtures were obtained and from these the required heat for evaporation could be estimated. During the dewatering process viscosity was monitored online and proved to be a sufficient and reliable indicator for dewatering progress.
Experimental and theoretical results on the flow pattern and film thickness of liquid falling films on the outside of a vertical pillow-type plate heat exchanger are presented. With the experimental setup, the wetting of a pillow plate and the local film thickness can be determined. The calculated mean film thickness is compared to literature data with an experimental investigation of a flat plate to assess the presented evaluation technique. Correlations for the mean film thickness on a flat plate and a pillow plate are given. The minimum flow rate per wetted length for a pillow plate is investigated.
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