Katrin Bode scite author profile

Tris(trimethylsilyl)hydrazin reagiert mit n‐BuLi in n‐Hexan zum Lithiumderivat 1. Reaktionen von 1 mit SiF4, PhSiF3, BF3 · OEt2, F2BN(SiMe3)2 und PF3 führen zu den Substitutionsprodukten 2–6. (Me3Si)2NN(SiMe3)BFN(SiMe3)2 (5) verliert thermisch Fluorsilan unter Bildung des 1,2‐Diaza‐3‐bora‐5‐sila‐cyclopentans 7. Bei der Umsetzung von (Me3Si)2NN(SiMe3)PF2 (6) mit lithiiertem tert.‐Butyl‐(trimethylsilyl)amin entsteht das Hydrazino‐Iminophosphen (Me3Si)2NN = PN(SiMe3)(CMe3) (8). Im molaren Verhältnis 2:1 reagiert 1 mit SiF4 zum Bis[tris(trimethylsilyl)hydrazino]silan 9 und mit BF3 · OEt2 zum Bis[tris(trimethylsilyl)hydrazino]boran.

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Lithium-bis(silyl)hydrazide, Tris(silyl)hydrazine und 1,2-Diaza-3,5-disilacyclopentane

Bode¹,

Drost²,

Jäger³

et al. 1994

Journal of Organometallic Chemistry

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Mono-, Bis-, Tris-, Tetrakis(silyl)hydrazine, Bis-Und Tris(hydrazino)silane: Synthese Und Kristallstrukturen

Bode

Klingebiel

Witte-Abel

et al. 1996

Phosphorus, Sulfur, and Silicon and the Related Elements

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Transglottic corticosteroid injection for treatment of soft post-intubation subglottic stenosis: a retrospective analysis of 26 children

Kaufmann

Bode

Puder

et al. 2019

Eur Arch Otorhinolaryngol

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Katrin Bode

Silylhydrazines: Lithium Derivatives Isomerism and Rings

Kristallstruktur des Bis[lithium‐tris(trimethylsilyl)‐hydrazids] und Reaktionen mit Fluorboranen, ‐silanen und ‐phosphanen

Lithium-bis(silyl)hydrazide, Tris(silyl)hydrazine und 1,2-Diaza-3,5-disilacyclopentane

Mono-, Bis-, Tris-, Tetrakis(silyl)hydrazine, Bis-Und Tris(hydrazino)silane: Synthese Und Kristallstrukturen

Transglottic corticosteroid injection for treatment of soft post-intubation subglottic stenosis: a retrospective analysis of 26 children

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