Oil droplet size distribution of an emulsion produced by Sulzer Chemtech's static SMX static mixer under flow condition was experimentally studied and reported. The dispersed phase of vegetable oil-in-water (O/W) emulsion produced through static mixer by varying the concentration from 1 to 4 vol % oil in water, flowrate of dispersed and continuous phase and operating time. The effect of run time on oil drop sizes is characterized using the spectra obtained from the particle size analyser. The static mixer with 9 perpendicular elements made of teflon is stacked against each other had a void fraction of 0.93. The sauter mean diameter of oil droplet decreases from 8 µm to 4 µm with an increase in Reynolds number. The emulsion droplets of mean sauter diameter in the range 4.1 µm to 4.7 µm were produced by increasing the concentration of the dispersed phase from 1:100 to 1:25, within a span value of between 30 to 240 sec, at atmospheric pressure and room temperature. Performance equation for sauter mean oil droplet diameter is developed based on the experimental data has ±0.2 rms deviation.
The effect of impeller clearance and liquid level on the critical impeller speed (Njs) for various radial and axial flow impellers in 0.29 m ID agitated vessel has been studied. Five types of radial impellers: Rushton turbine (RT), Straight blade (SB), Curved blade (CB), Curved blade with disc (CBWD) and R130 impeller and four types of axial impellers: Rushton turbine 45 o angle (RT 45), Pitched blade (PBT), A320 and HE3 impeller were used. Tap water and resin particle of 0.506 mm were used as liquid and solid phases, respectively. The impeller clearance to vessel diameter (T) was varied between 0.17 and 0.41. The liquid level (H) was also varied as H/T=0.5, H/T=0.75 and H/T=1. The R130 impeller and A320 impeller was found to be more efficient among radial and axial impellers respectively. A new expression for Zwietering constant 'S' was developed to predict critical impeller speed, considering impeller clearance and liquid level for all the impellers. The results obtained here show that the 'S' values increase with increase in clearance, and decrease with liquid level for all impellers and it also depends on the type of impeller.
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