Crato Formation, NE Brazil, consists of laminated limestones deposited in a lacustrine environment during the Early Cretaceous. The Nova Olinda Member, the lowest unit of the Crato Formation, is world-famous for their exceptionally well-preserved fossils. The Nova Olinda limestones have been economically exploited for centuries. Today, this commercial excavation still represents the main economic activity in the region. During the mining process, the quarry workers have developed an informal stratigraphic code to individualize the different beds in the quarries. Upward, the local workers recognize the succession as “lajão dos sete cortes”, “matracão", “lajão branco", “pão de milho”, “veio da paiba”, "veio doidão”, “lajão amarelo” and “veio do besouro”. Here, we used principles of ethnostratigraphy to verify the origin and validity of these informal stratigraphic nomenclatures by classifying them as ethnostra. For this, we applied a detailed petrographical analysis with thin sections and high-resolution X-ray techniques to characterize each ethnostratum. Our results suggest possible linkages between informal and formal stratigraphic nomenclatures in Nova Olinda Member. Finally, this study showed that ethnostratigraphy can be applied as an auxiliary tool in stratigraphic studies, in both, as an initial exploratory approach and as enhancing the relationship between the geologists and the local community.
Growth in the international popularity of Brazil nuts oil (Bertholletia excelsa, Bonpl.) has demanded a closer look at quality aspects of the nuts. In this context, time-domain 1H nuclear magnetic resonance spectroscopy (TD-NMR) can be a useful tool for assessing the lipid portion of such matrices. In this work, a TD-NMR method was developed and validated to assess the oil content directly from Brazil nuts following the ISO 10565:1998 and DOQ-CGCRE-008. Full validation was addressed covering the working range from 0.67 to 25.00 g (coefficient of determination, R2 = 0.9993). Limits of detection (LOD) and quantification (LOQ) were 0.20 and 0.67 g, respectively. The repeatability and intermediate precision assays met the guide requirements. Oil contents obtained in two laboratories (different equipment) were statistically similar (66.93 ± 4.69 and 70.13 ± 4.15%), highlighting the method’s robustness. The developed approach has the potential to be adopted as an industrial reference method for in situ monitoring of Brazil nuts oil contents.
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