Statement of problem. One-step and incremental mixing procedures are currently used to produce dental ceramic pastes. In the ceramic industry, high quality is obtained using one-step mixing, but in dentistry, the best method has not been yet determined.Purpose. The purpose of this study is to evaluate the effects of 2 mixing techniques on the biaxial flexural strength and microstructure of dental porcelain. Material and methods.Feldspathic porcelain discs (2 x 15 mm in diameter) were produced and divided according to the ceramic paste preparation method, powder-liquid incremental mixing group (n=50) or one-step mixing, as a control group (n=50). Specimens were tested for biaxial flexural strength and characterized using porosimetry, relative humidity, SEM/EDS, XRD, and F T-IR analyses. Statistical analysis was conducted using Weibull statistics. The Weibull modulus, characteristic strength and relative humidity were compared between groups, using Student's t-test and Mann-Whitney U test (α=.05).Results. The powder-liquid incremental mixing group showed significantly higher values (SD) of Weibull modulus (6.74 (0.70), P<.001) and characteristic strength (79.87 (2.01) MPa, P<.001) when compared to the one-step mixing group (4.94 (0.94) and 75.95 (2.61) MPa). Significantly lower mean (SD) relative humidity values (P=.009) were found for powder-liquid incremental mixing group (20% (0.5%)) compared to one-step mixing group (22% (1%)). XRD spectra showed that the one-step mixing group produced higher amounts of the amorphous phase. Conclusions.Specimens produced by the incremental mixing technique showed higher biaxial flexural strength than one-step mixing. (J Prosthet Dent 2011;105:308-314)
Background. The ceramics industry produces porcelain pastes using a controlled ratio of water and porcelain powder. Two methods are used to produce a dental porcelain paste: one-step mixing or incremental mixing. Objective. To evaluate the optical properties of a feldspathic dental ceramic using two different ceramic paste preparation methods using a Bayesian approach. Materials and Methods. Two groups of feldspathic porcelain discs, an incremental mixing group (n = 40) and a one-step mixing group (n = 40), were assessed. Groups were evaluated using spectrophotometry, and the translucency parameter (TP) of each sample was calculated. Surfaces were characterized by AFM and SEM. Statistical analysis was performed using a Bayesian approach. Results. Translucency parameter values of the incremental mixing group ranged from 1.65 to 3.41, while values for the one-step mixing group ranged from 3.62 to 5.74, this difference being statistically significant. The lowest roughness was obtained on the surface of discs in the one-step mixing group. Conclusions. Feldspathic porcelain with lower translucency and higher roughness was obtained using the incremental mixture method.
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