Polymethyl methacrylate (PMMA) is one of the common widely accepted biomaterials in prosthetic dentistry due to its acceptable advantages, since 1937. In the present work, PMMA reinforced with Al2O3 nanowires (Al2O3 NWs) and ZrO2 nanoparticles (ZrO2 NPs) were fabricated by a self-curing method. Mechanical and tribological tests were conducted to study the effect of nanofillers on the mechanical and tribological performance of PMMA nanocomposites. Compression and microhardness tests, as mechanical tests, were accomplished to estimate the elastic modulus and microhardness number of the present nanocomposites. Also, tribological properties of unfilled PMMA and its nanocomposites were realized by pin-on-disk tester under dry sliding conditions. Wear test was conducted at room temperature under applied loads of 10, 20, 30, 40, and 50 N at a constant sliding speed and distance of 1.256 m/s and 226 m, respectively to study wear rate and coefficient of friction (COF) of the nanocomposites. Experimental results revealed that the elastic modulus, microhardness, wear rate, and COF were enhanced with increasing nanofiller content up to 0.5 and 0.7 wt. % of Al2O3 NWs and ZrO2 NPs, respectively. Also, wear rate increased with increasing applied loads up to 50 N, while COF decreased with increasing applied loads up to 40 N. Finally, specimens� worn surfaces were examined and imaged using scanning electron microscope (SEM).
This study aims to investigate the impact of partial-contact tool tilt angle (TTA) on the mechanical and microstructure properties of the AA1050 alloy friction stir weld (FSW). Three levels of partial-contact TTA were tested, 0°, 1.5°, and 3°, compared to previous studies on total-contact TTA. The weldments were evaluated using surface roughness, tensile tests, microhardness, microstructure, and fracture analysis. The results show that in partial-contact conditions, increasing TTA decreases the generated heat in the joint line and increases the possibility of FSW tool wear. This trend was the opposite of joints that were friction stir welded via total-contact TTA. The microstructure of the FSW sample was finer at higher partial-contact TTA, while the possibility of defect formation at the root of the stir zone in higher TTA was more than in lower TTA. The robust sample prepared at 0° TTA had 45% of AA1050 alloy strength. The maximum recorded heat in 0° TTA was 336 °C and the ultimate tensile strength of this sample was 33 MPa. The elongation of the 0° TTA welded sample was 75% base metal, and the average hardness of the stir zone was 25 Hv. The fracture surface analysis of the 0° TTA welded sample consisted of a small dimple, indicating the brittle fracture mode.
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