The mass transfer coefficient between fluid and an immersed sphere in liquid packed and fluidized beds of inert spherical particles have been studied experimentally using a column 40 mm in diameter. The mass transfer data were obtained by studying the transfer of benzoic acid from the immersed sphere to flowing water using the dissolution method. In all runs, the mass transfer rates were determined in the presence of inert glass particles 0.50-2.98 mm in diameter. The influence of different parameters, such as: liquid velocity, particles size and bed void age, on the mass transfer in packed and fluidized beds is presented. The obtained experimental data for mass transfer in the packed and particulate fluidized bed were correlated by a single correlation, thus confirming the similarity between the two systems.

Izvod U ovom radu prikazani su rezultati eksperimentalnih ispitivanja prenosa količine kretanja, toplote i mase zid-fluid u vertikalnom hidrauličkom transportu inertnih čestica i pri strujanju fluida u cevi istog prečnika. Eksperimentalna ispitivanja vršena su istovremenim merenjem potrebnih parametara za definisanje navedenih prenosa. Cilj ovih ispitivanja bio je određivanje koeficijenata prenosa pri vertikalnom hidrauličkom transportu inertnih čestica i uspostavljanje analogije tri prenosa. Eksperimentalni sistem predstavljala je vertikalna transportna cev prečnika 25,4 mm snabdevena omotačem za zagrevanje parom, kao i segmentom transportne cevi prepariranim rastopom benzoeve kiseline. Kao fluid korišćena je voda, a vršen je transport staklenih sfernih čestica prečnika 1,94 mm. U rezultatima su prikazani dobijeni koeficijenti trenja, prelaza toplote i prelaza mase. Korišćenjem koncepta pseudofluida, pokazano je postojanje analogije prenosa količine kretanja, toplote i mase u transportnoj cevi za paralelni režim strujanja.

ABSTRACT:The aim of this study was to find an optimal way of tomato drying in a tunnel type dryer, in order to achieve the lowest possible losses in nutritive value of dried tomato products. Domestic variety of tomato (SP-109) was used in this research. Drying was performed in three ways, applying five temperature regimes, as follows: cocurrent system (variant 1 at 70- . In these systems, the kinetic of changes in nutritive value of tomato fruits was monitored by measuring the content of carbohydrates, lycopene and vitamin C. Different influences of temperature regimes on nutritive value of dried tomato were observed at the level of statistical difference (LSD 0.05; 0.01) in the researched systems. Cocurrent system was statistically significant for differences in temperature modes (variant 1 and variant 2). Monitoring of the tomato drying kinetics showed that, in all variants, period of constant drying rate lasted about 3.5 h and that the total drying was the fastest in parallel cocurrent flow of non-saturated hot air and material. The content of total carbohydrates in tomato was dependent on the temperature regime of the tested drying systems. The carbohydrate content obtained in tomato samples dried at lower temperatures was higher compared to the values observed in the samples dried at higher drying temperatures. Significant losses of vitamin C were determined in all drying systems. The lycopene content under all experimental conditions generally showed a tendency to decrease slightly. Comparing its content in dry and fresh tomato fruits, the loss ranged from 4.94% to 19.98% but did not reach the significant level as the occurrence remained below 95% of cases.

Mass transfer in fluidized beds is an important operation for separation processes. Two effects can be achieved by using fluidized beds in mass transfer processes increasing interface area and relative movement between the phases. These effects are both desirable because they lead to greater process rates. This paper presents an experimental investigation regarding mass transfer from the wall of a column to the fluid in a fluidized bed of inert spherical particles. The experiments were conducted in column 40 mm in diameter with spherical particles 0,8-3 mm in diameter and water as one fluidizing fluid. The method of dissolution of benzoic acid was used to provide very low mass flux. The average wall-to-fluid mass transfer coefficients were determined for two systems: single-phase fluid flow and a fluidized bed of inert particles The measurements encompassed a Reynolds number range from 100-4000 for single-phase flow and 600-4000 in fluidized beds. The mass transfer coefficients for both systems were calculated from weight loss of benzoic acid. The effects of superficial liquid velocity and particle diameter on the mass transfer coefficient were investigated. It was found that mass transfer was more intensive in the fluidized bed in comparison with single phase flow. The best conditions for mass transfer were reached at a minimum fluidization velocity, when the mass transfer coefficient had the greatest value. The experimental data were correlated in the form: jd = f(Re), where jd is the dimensionless mass transfer factor and Re the Reynolds number