In this letter, we address the relationship between the statistical fluctuations of grain displacements for a full quasistatic plane shear experiment, and the corresponding anomalous diffusion exponent, α. We experimentally validate a particular case of the so-called Tsallis-Bukman scaling law, α = 2/(3 − q), where q is obtained by fitting the probability density function (PDF) of the measured fluctuations with a q-Gaussian distribution, and the diffusion exponent is measured independently during the experiment. Applying an original technique, we are able to evince a transition from an anomalous diffusion regime to a Brownian behavior as a function of the length of the strain-window used to calculate the displacements of grains in experiments. The outstanding conformity of fitting curves to a massive amount of experimental data shows a clear broadening of the fluctuation PDFs as the length of the strain-window decreases, and an increment in the value of the diffusion exponent -anomalous diffusion. Regardless of the size of the strain-window considered in the measurements, we show that the Tsallis-Bukman scaling law remains valid, which is the first experimental verification of this relationship for a classical system at different diffusion regimes. We also note that the spatial correlations show marked similarities to the turbulence in fluids, a promising indication that this type of analysis can be used to explore the origins of the macroscopic friction in confined granular materials. Turbulence is one of the most complex, but ubiquitous, phenomena observed in Nature and it is related with the underlying mechanisms responsible for the micro-macro upscale causing wide-ranging effects on classical systems, like macroscopic friction in granular solids or turbulent flow regime in fluids [1][2][3][4]. The presence of multiple scales in time and space is an additional defy to a comprehensive theoretical description, and a particular effort is made in the literature to perform experiments and simulations in order to validate the proposed theoretical descriptions, particularly Tsallis nonextensive (NE) statistical mechanics [5][6][7][8].A paradigmatic work relating anomalous diffusion and turbulent-like behavior in confined granular media was presented by Radjai and Roux [4], using numerical simulations, and confirmed qualitatively by experiments by Combe and collaborators [7,8]. Radjai and Roux coined a new expression to characterize the analogies between fluctuations of particle velocities in quasistatic granular flows and the velocity fields observed in turbulent fluid flow in high Reynolds number regime, the "granulence". Most of the evidences of the granulence are based in simulations using discrete element method (DEM) but, unfortunately, one can verify a lack of quantitative experimental verification in the last years, limiting the knowledge of the micromechanics of this system based almost exclusively on numerical evidences.In the present work, we aim exactly to fill this gap by contributing with the experiment...

We focus herein on the mechanical behavior of highly crushable grains. The object of our interest, named shell, is a hollow cylinder grain with ring cross-section, made of baked clay. The objective is to model the fragmentation of such shells, by means of discrete element (DE) approach. To this end, fracture modes I (opening fracture) and II (in-plane shear fracture) have to be investigated experimentally. This paper is essentially dedicated to mode I fracture. Therefore, a campaign of Brazilian-like compression tests, that result in crack opening, has been performed. The distribution of the occurrence of tensile strength is shown to obey a Weibull distribution for the studied shells, and Weibull's modulus was quantified. Finally, an estimate of the numerical/physical parameters required in a DE model (local strength), is proposed on the basis of the energy required to fracture through a given surface in mode I or II.

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