This paper presents the results of an interlaboratory study of the rheological properties of cement paste and ultrasound gel as reference substance. The goal was to quantify the comparability and reproducibility of measurements of the Bingham parameters yield stress and plastic viscosity when measured on one specific paste composition and one particular ultrasound gel in different laboratories using
Rheological properties of cementitious suspensions are affected not only by their mixture composition but also by process-related factors such as shear history. To enable a model-based description, investigations were carried out on the effect of shear history (shear rate variation over time) on the cement paste agglomeration state. Therefore, a Focused Beam Reflectance Measurement (FBRM) system and a wide gap rheometer were coupled to study the relation between shear history and in-situ chord length distribution simultaneously, indicating particle agglomeration. Hence, the effect of average shear rates (resulting from the applied shear profile), as well as shear rate distribution within the gap (local shear rates) on the particle agglomeration state have been investigated. The rheological properties of cement paste were evaluated with the Reiner–Riwlin approach. Furthermore, the agglomeration state of the particles was compared for different average shear rates and local shear rates at various positions of the FBRM probe. The results show that the median chord length increases in all positions when the average shear rate is decreased, indicating increasing particle agglomeration. Moreover, due to variable local shear rates at different FBRM probe positions, different agglomeration states are observed, resulting from two factors, shear rate dependent particle agglomeration and shear-induced particle migration.
The modeling of fresh concrete flow is still very challenging. Nevertheless, it is of highest relevance to simulate these industrially important materials with sufficient accuracy. Often, fresh concrete is assumed to show a Bingham-behavior. In numerical simulations, regularization must be used to prevent singularities. Two different regularization models, namely the 1) Bi-viscous, and 2) Bingham-Papanastasiou are investigated. Those models can be applied to complex flows with common simulation methods, such as the Finite Volume Method (FVM), Finite Element Method (FEM) and Smoothed Particle Hydrodynamics (SPH). Within the scope of this investigation, two common software packages from the field of FVM, namely Ansys Fluent and OpenFOAM, COMSOL Multiphysics (COMSOL) from FEM side, and HOOMD-blue.sph from the field of SPH are used to model a reference experiment and to evaluate the modeling quality. According to the results, a good agreement of data with respect to the velocity profiles for all software packages is achieved, but on the other side there are remarkable difficulties in the viscosity calculation especially in the shear- to plug-flow transition zone. Also, a minor influence of the regularization model on the velocity profile is observed.
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