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3 ,Z=2,

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C 14 H 17 N 3 O 2 , monoclinic, P2 1 /c (no. 14), a = 14.9289(7) Å, b = 7.8070(4) Å, c = 12.4664(7) Å, CCDC no.: 1572566The crystal structure is shown in the figure. Tables 1 and 2 contain details on crystal structure and measurement conditions and a list of the atoms including atomic coordinates and displacement parameters. Source of materialThe title compound was obtained using the synthetic method described earlier [5,6]. A mixture of dimethylaniline (7.24 mmol) in 4.5 mL of HCl/water (1:1) was cooled at 0-5°C and added dropwise a solution of sodium nitrite 525 mg (7.60 mmol) in 30 mL of water. The resulting mixture was stirred for 10 min, then it was slowly added a solution of sodium azide (612 mg, 9.41 mmol) in 60 mL of cold