<p>Deformation bands, or tabular zones of localised strain, are a common manifestation of deformation in upper crustal sedimentary rocks. Any mining or energy-related engineering applications must consider the possibility of reactivating these pre-existing failure planes because doing so can cause seismicity and compartmentalise the reservoir. However, there has only been a small amount of research done on laboratory-induced deformation in rocks with natural deformation features.</p><p>On a low porosity bioclastic calcarenite from the Cotiella Basin, Spanish Pyrenees, our current experimental work aims to capture, for the first time to our knowledge, the dominant failure mechanisms during the reactivation of natural deformation bands oriented at different angles to the principal stress direction. At the I12-JEEP beamline at the synchrotron facility of Diamond Light Source, UK, we carried out triaxial compression experiments using a modified version of the Mjolnir cell used by Cartwright-Taylor et al., (2022) to examine how these highly heterogeneous rocks respond to additional mechanical deformation. During the deformation experiments, 4D (time and space) x-ray tomography images (8 m voxel size resolution) were acquired. We tested confining pressures between 10 MPa and 30 MPa.</p><p>The mechanical data demonstrate that the existence of natural deformation features within the tested samples weakens the material. For instance, solid samples of the host rock subjected to the same confining pressures had higher peak differential stresses. Additionally, our findings demonstrate that new deformation bands form as their angle, θ, to σ1 increases, while the reactivation of pre-exiting deformation bands in this low porosity carbonate only occurs for dipping angles close to 70<sup>o</sup>. The spatio-temporal relationships between the naturally occurring and laboratory-induced deformation bands and fractures were investigated using time-resolved x-ray tomography and Digital Volume Correlation (DVC). Volumetric and shear strain fields were calculated using the SPAM software (Stamati et al., 2020). The orientation of the recently formed failure planes is influenced by the orientation of the pre-existing bands, as well as their width and the presence (or absence) of porosity along their length. Additionally, pre-existing secondary deformation features found in the tested material trigger additional mechanical damage that either promotes the development or deflects the new failure planes.</p><p>References</p><p>Cartwright-Taylor et al. 2022, Nature Communications 13, 6169, https://doi.org/10.1038/s41467-022-33855-z</p><p>Stamati et al. 2020, Journal of Open Source Software, 5(51), 2286, https://doi.org/10.21105/joss.02286</p>

<p>Reservoir rocks, such as carbonates, are rapidly becoming key elements for the energy transition. The damage of these reservoir rocks when placed under a stress field must be characterized, to better predict storage capacity distribution. In the shallow subsurface, carbonate rocks accommodate the stress by developing structures at the mesoscale, such as fractures, deformation bands or stylolites, depending on porosity or fluid content. Those are localized, showing a finite damaged area, outside which the relative host rock can accommodate the applied stress in a different way, usually overlooked in low temperature and pressure conditions.</p> <p>In this study, we highlight a new marker of accommodation of shortening, characterized by heterogeneous quartz grain rotation in non-porous carbonate matrix. The studied rock is an upper Cretaceous bioclastic calcarenite from the Cotiella Massif (Spain). This rock is composed of 85% carbonate (micrite and recrystallized microsparite), 10% quartz, and <5% of nanometric porosity. It hosts a fracture pattern including fractures, stylolites and deformation bands that correspond to different tectonic stages. However, we focus on investigating the quartz grain orientation in the grains outside the deformation bands, in both the far-field and near-field host rock. We investigated the fabric (typology, distribution and orientation) of thousands of quartz grains using X-ray microtomography on cylindrical cores of 8-26 mm diameter. Each segmented quartz grain is approximated with a best-fit ellipsoid whose major axis (L1) and minor axis (L3) give us information about the average orientation of the quartz grain. We show that the typology of the quartz grains, namely the size and average shape is similar in all our samples.</p> <p>The average orientation of all quartz grains at the core scale reveals subtle preferences, without clear correlation to the orientation of neither the stylolites nor the deformation bands. We observe that in half of the samples studied, the quartz grain fabric is not controlled by the bedding. Instead, there are two distinct patterns of grain orientation, with the quartz grain fabric either reflecting the early burial stage or revealing a later reorientation perpendicular to one of the major shortening directions. These directions are either striking parallel to the local shortening flow (NE-SW) or to the regional orogenic flow (N-S), that is attributed to the Pyrenean orogeny. Evidence of dissolution-recrystallization are observed in quartz, but the diagenetic conditions constrainthis mechanism from being a robust hypothesis to explain the change of quartz fabric, but rather favour the rigid rotation of quartz in a micritic matrix. The examination of both the quartz grains and the carbonate matrix with EBSD suggests a local strain accumulation within the carbonates in the vicinity of quartz grains. Although the mechanisms causing this rotation need to be better understood, measuring the grain typology and orientation on a considerable number of grains with the aid of X-ray microtomography could result in a new method of deformation quantification in carbonate rocks.</p>

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<p>We report for the first time deformation features functionally described as deformation bands developed in low porosity rocks. This observation contradicts existing knowledge that deformation bands develop only in highly porous rocks. The studied formation is a bioclastic calcarenite of the Upper Cretaceous Maciños Unit in the Cotiella Massif. It is part of a megaflap adjacent to a salt diapir that has experienced extensional tectonics before the Pyrenean contraction. The bands present thickness variations, and in places they imitate the appearance of stylolites. This observation raises the question: how do deformation bands form in low porosity rocks?</p><p>To answer the question, we combine field observations with microstructural analysis to identify the occurring processes for the formation of deformation bands within low porosity rocks. After using optical microscopy and cathodoluminescence spectroscopy to conduct a petrographic study, we observe that the rock underwent multiple diagenetic cycles before the deformation stage, confirming that its porosity was significantly reduced before the deformation stage. Subsequently, we characterized the quartz grains inside the host rock and the dissolution-enabled deformation bands, using non-destructive imaging techniques. Three-dimensional image analysis from X-ray microtomography scans shows low grain size variations between the quartz grains in the host rock and in the bands, suggesting minor grain fracturing along the bands. However, grain reorientation has been reported for the quartz grains inside the bands, in relation to those in the host rock. Strain analysis was performed from Electron Backscattered Diffraction measurements, revealing higher strain along the quartz grain contacts inside the deformation band, compared to those in the host rock and stylolites. Our current data suggest that new porosity was created from local dissolution of the matrix, so the less soluble quartz grains were placed in contact. By wrapping-up the above observations, we propose a conceptual model that demonstrates the genesis and evolution of dissolution-enabled deformation bands in low porosity rocks, through local dissolution of the micritic matrix and transient porosity increase.</p>