Sample calculationSample size was calculated in terms of a minimum detectable difference in a mean BS (Mpa) of 0.62 (30 human teeth, 8 per group), using the same adhesive system with and without enamel acid etching. 2 However, for predicting eventual losses, 11 samples (10 stick each, on average) were included. Specimen preparationThe crown from each tooth was sectioned in the bucal-lingual direction using a 4 "x 0.012" x 0.5 "diamond cutting disc (Erios Equipamentos Ltda -EPP, São Paulo, Brazil) mounted in a precision
RESUMO:Quanto menor a superfície da área, maior a resistência de união, pois, espécimes com pequena área de superfície apresentam melhor distribuição de estresse, bem como reduzido número de defeitos internos. O objetivo deste estudo foi verificar a resistência de união ao microcisalhamento de espécimes com dois diferentes diâmetros, 0.55 mm e 0.76 mm. 40 fatias de cerâmica Suprinity, com 1,3 mm de espessura, polidas em lixa #600, foram divididas aleatoriamente em dois grupos (n=20). Em cada fatia, quatro áreas adesivas foram delimitadas por fita adesiva, sendo então fixadas as matrizes circulares. Os espécimes foram condicionados com ácido fluorídrico a 5% (FGM) por 20 s, lavados e secos; então silanizados (RelyX Ceramic Primer -3M ESPE) e secos com jato de ar. As matrizes foram preenchidas com cimento resinoso RelyX U200 3M ESPE e fotopolimerizadas por 100 s. Após 24 h em água deionizada a 37 o C, os espécimes foram submetidos ao teste de microcisalhamento sob velocidade de 0,5 mm/min. Os dados normais e homogêneos foram submetidos à ANOVA para o experimento inteiramente casualizado, não exibindo diferença significativa (p =0,62) entre as duas áreas avaliadas -23,74±4,49 e 24,85±4,41, respectivamente para as áreas 0,55 e 0,76 mm. Concluímos que, não há diferença na resistência de união ao microcisalhamento quando se utilizam as diferentes áreas adesivas estudadas. PALAVRAS-CHAVE:Resistência ao cisalhamento; Adesivos; Cerâmicas. DIFFERENT ADHESIVE AREAS AFFECT RESISTANCE TO MICRO-SHEARING BONDING?ABSTRACT: The smaller the surface area, the greater is the resistance. Specimens with small surface area have a better stress distribution and a reduction in the number of internal faults. Bonding resistance to micro-shearing of specimens with two different diameters, 0.55 mm and 0.76 mm, were analyzed. Forty Suprinity ceramic slices, 1.3 mm thick, polished by file #600, were randomly divided into two groups (n=20). Four adhesive areas in each slice were delimited by adhesive tape and fixed to circular matrixes. Specimens were conditioned with hydrofluoric acid 5% (FGM) for 20 s, washed, dried, silanized (RelyX Ceramic Primer -3M ESPE) and dried by air jet. Matrixes were filled with resinous cement RelyX U200 3M ESPE and photopolymerized for 100 s. After 24 h in de-ionized water at 37 o C, the specimens underwent micro-shearing test at 0.5 mm/min. Normal and homogeneous data were submitted to ANOVA for totally randomized assay, with no significant difference (p=0.62) between the two areas under analysis -23.74±4.49 and 24.85±4.41, respectively for areas 0.55 and 0.76 mm. Results show that no bonding resistance to micro-shearing exists when different adhesive areas are employed.
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