Synthesis of BiFeO3-BaFe12O19 solid solution is aimed to enhanced magnetic properties of the material which can improve the quality of multiferroic properties of material. As we know that BiFeO3 is a multiferroic material if it is in single phase but unfortunately it is difficult to produce BiFeO3 in single phase, which can cause a large current leakage arising from non stoichiometric. It used sol gel method to produce BiFeO3-BaFe12O19 solid solution with weight ratio of 1;1. To know magnetic properties, it was used permagraph test which is type of MPS magnet – Physic EP3 – Permagraph L . The sintering temperature was 750, 800 and 850oC for 8, 10 and 12 hours respectively. There is no regularity in increasing and decreasing of remanent and coersivity properties with increasing sinter temperatures and time of sintering but there is an increasing magnetic energy with increasing sinter temperatures and time of sintering. The highest value of magnetic energy, 10.716 GkA/m belongs to powder sintered at 850oC for 12 hours.
Aluminium paduan Al-Mg-Si khususnya T6061 merupakan paduan yang pada umumnya diaplikasikan untuk otomotif dan alat-alat konstruksi. Penelitian ini diarahkan untuk peningkatan sifat mekanis khususnya kekerasan material T6061 untuk diaplikasikan sebagai selongsong peluru. Selama ini material untuk selongsong peluru banyak menggunakan kuningan yang mempunyai density yang lebih besar daripada aluminium padahal sebagai selongsong peluru diperlukan material yang ringan tetapi kuat sehingga dapat menembakan peluru dengan lancar dan mudah. Untuk peningkatan sifat mekanis dilakukan perlakuan panas precipitation hardening melalui proses pemanasan pada temperatur 500oC selama 1 jam kemudian dicelup di dalam air sampai mencapai temperatur kamar, setelah itu untuk peningkatan kekerasan dilakukan proses aging (penuaan) pada temperatur 90, 120, 150, 180 dan 210oC masing-masing selama 8,9 dan 10 jam. Karakterisasi aluminium setelah mengalami precipitation hardening adalah dengan melakukan pengujian kekerasan metode Vickers dan pengamatan struktur mikro. Dari hasil pengujian kekerasan diperoleh hasil bahwa kekerasan terus meningkat mulai dari temperatur aging 90oC sampai dengan temperatur aging 150oC. Kekerasan maksimum diperoleh pada temperatur aging 150oC sebesar 103 HV. Di atas temperatur 150oC terjadi penurunan kekerasan yang menandakan bahwa terjadi over aging pada temperatur di atas 150oC yang ditandai dengan makin membesarnya presipitat Mg2Si. Kondisi aging optimum yang dapat diterapkan untuk precipitation hardening T6061 yang diaplikasikan untuk selongsong peluru adalah temperatur aging 150oC selama 8, 9 dan 10 jam.
The nanomultiferroic material which is synthesized in this research used sol-gel method. The research used weight ratio of BaTiO3: BiFeO3 of 2: 1. Gel formed after heating at 80-90°C was calcined at 350°C for 4 hours and then sintered at 700,750 and 800°C for 2, 4 and 6 hours respectively. Powder produced after sintering was characterized by X-Ray Diffraction (XRD) test using XRD Phillips PW 1835 type, 20°-100° diffraction angle and CuKα, electric polarization properties test and particle size measurement using Particle Size Analyzer of Beckman Coulter DelsaTM Nano instrument. From the characterization results, it is obtained that the dominant phase is Barium Bismuth Iron (III) Oxide (BaBiFe2O5). Electrical polarization properties such as remanent, coersivity and saturation reach maximum value at sinter temperature of 750° C and sinter time of 6 hours. This result is supported by the smallest particle size of powder (54-57 nm) and also supported by the largest number of dominant phase (98.79%) at same condition.
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