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Table of contents 1. Analytical instrumentation 3 2. Synthetic protocols 4 2.1. General synthetic procedures 4 2.2. Synthetic procedures for LCs 5 2.3. Synthetic procedures for single-ring model molecules 3. Phase transition temperatures and enthalpies 3.1. Liquid crystalline precursors of deuterated LCs 3.2. Deuterated LCs 4. 1 H NMR and 13 C NMR for 2T3 family 5. DSC analysis 6. Fragmentation paths and mass spectra for model compounds 7. Photodegradation -DSC analysis 8. GC-MS analysis and mass spectra for photodegradation products

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