The popular superalloy Alloy 625 was produced by Selective Laser Melting (SLM) and post-processing heat treatments were designed to optimize the inhomogeneous and constrained as-built microstructure (AB) for high temperature structural applications. A single-step solution heat treatment (RX) was designed to promote full recrystallization and approach the conventional wrought microstructure. To enhance high temperature properties, a grain boundary serration heat treatment (GBS) was successfully designed involving higher solution temperature and time to promote recrystallization and homogeneity, and a direct slow cooling step followed by a short aging to assist solute diffusion and grain boundary motion. The resulting microstructures were characterized by fully recrystallized fine equiaxed grains and fine intra and intergranular NbC precipitates. The GBS alloy also exhibited as much as 80% of serrated grain boundaries with enhanced resistance to cracking at high temperatures. Tensile properties of all three materials were evaluated at room temperature, 500 � C, 600 � C and 700 � C and compared with their conventional solutionized wrought Alloy 625 counterpart (Wrought). While the AB material exhibited high strength and low ductility, due for the most part to the high density of tangled dislocations resulting from SLM, both RX and GBS alloys showed tensile properties comparable to the conventional wrought material, higher strength in particular. At all temperatures, all four alloys exhibited yield strength values well over 200 MPa. Due to significantly different microstructures, deformation and fracture behaviors were different. While Wrought clearly presented irregular plastic flow at elevated temperatures typically attributed to dynamic strain aging (DSA), the materials produced by SLM and moreover those subjected to postprocessing heat treatments exhibited more stable plastic deformation. The results and characterization reported in the present article highlight the predominant role of microstructure and outstanding potential of SLMed Alloy 625.
Third generation γ‐TiAl alloys with a high niobium content, Ti–(47–48)Al–2Cr–8Nb, were processed by electron beam melting (EBM). This near‐net‐shape additive manufacturing process produces complex parts according to a CAD design. The starting powder is deposited layer by layer on the building table and selectively melted to progressively form the massive part. The EBM parameters such as layer thickness, melting temperature, scanning speed, or building strategy were set up to minimize porosity. The chemical composition of the built material is similar to the composition of the base powder despite a slight evaporation of aluminum and reveals a neglectable oxygen pick‐up. The very fine equiaxed microstructure resulting after EBM can be then set up by heat treatment (HT). According to the HT temperature in particular, an equiaxed microstructure, a duplex microstructure with different lamellar ratio and a fully lamellar microstructure is obtained. Not only test bars have been produced but also complex parts such as demo low pressure turbine blades.
To improve the corrosion-resistant properties of carbon steel cladding process is usually used. It is a process of depositing a thick layer of corrosion resistant material-over carbon steel plate. Most of the engineering applications require high strength and corrosion resistant materials for long-term reliability and performance. By cladding, these properties can be achieved with minimum cost. The main problem faced in cladding is the selection of optimum combinations of process parameters for achieving quality clad and hence good clad bead geometry. This paper highlights an experimental study to optimize various input process parameters (welding current, welding speed, gun angle, contact tip to work distance, and pinch) to get optimum dilution in stainless steel cladding of low-carbon structural steel plates using gas metal arc welding (GMAW). Experiments were conducted based on central composite rotatable design with full-replication technique and mathematical models were developed using multiple regression method. The developed models have been checked for adequacy and significance. Using particle swarm optimization (PSO) the parameters were optimized to get minimal dilution.
The present study investigated for the first time the feasibility of producing by Selective Laser Melting (SLM) a NiCrAlY bond coat material directly onto an IN625 substrate itself produced by SLM. A typical parameters optimization was conducted by varying laser power (P) and scanning speed (v). Single-line scanning tracks and two-layer coatings were carried out and analyzed for 15 different P/v conditions. Several criteria were defined for the selection of appropriate SLM parameters. The results showed significant remelting of the underlying substrate, which is a typical feature of SLM manufacturing. This led to the formation of an intermediate dilution zone characterized by substantial mixing between IN625 superalloy substrate and NiCrAlY bond coat suggesting excellent metallurgical bonding. Optimum processing conditions were found for P = 250 W and v = 800 mm/s. It produced a dense 242 μm thick bond coat including a 36% dilution zone. The SLMed < NiCrAlY-IN625 > system exhibited a smooth microhardness profile slightly increasing from 275 Hv in the bond coat to 305 Hv in the substrate. A progressive Al concentration distribution between the phases and low residual stress levels were found in the system. This suggested that SLM might be a valuable alternative manufacturing process for bond coat systems promoting excellent adhesion for high temperature applications.
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