A sound understanding of the water permeability evolution in fractured shale is essential to the optimal hydraulic fracturing (reservoir stimulation) strategies. We have measured the water permeability of six fractured shale samples from Qiongzhusi Formation in southwest China at various pressure and stress conditions. Results showed that the average uniaxial compressive strength (UCS) and average tensile strength of the Qiongzhusi shale samples were 106.3 and 10.131 MPa, respectively. The nanometre-sized (tiny) pore structure is the dominant characteristic of the Qiongzhusi shale. Following this, we proposed a pre-stressing strategy for creating fractures in shale for permeability measurement and its validity was evaluated by CT scanning. Shale water permeability increased with pressure differential. While shale water permeability declined with increasing effective stress, such effect dropped significantly as the effective stress continues to increase. Interestingly, shale permeability increased with pressure when the pressure is relatively low (less than 4 MPa), which is inconsistent with the classic Darcy's theory. This is caused by the Bingham flow that often occurs in tiny pores. Most importantly, the proposed permeability model would fully capture the experimental data with reasonable accuracy in a wide range of stresses.
In order to explore the deterioration mechanism of mechanical properties of phosphate rock under different saturation time, the degradation mechanism of phosphoric rock samples under different saturation duration was analyzed by laboratory test, theoretical analysis and neural network modeling, and the results is as follows: saturation of water will result in deterioration of mechanical properties of samples. The peak compressive strength and peak strain of the samples decreased gradually with the increase of saturation time. The average peak strength of 12, 24, and 36 h saturated specimens is 8.6%, 21.1%, and 32.2% lower than that of natural specimens, and the peak strain is 5.9%, 13.9%, and 31.3% lower, respectively. The stress-strain curves of the samples with water saturation for 36 h have more jitter stages after the peak, indicating that the plastic characteristics of the samples will be increased with water saturation for a long time. The neural network method was used to analyze the test parameters and the mechanical parameters of the samples, and the mechanical properties under the action of saturated water and confining pressure were obtained. The neural network model was established to represent the mechanical properties of the samples, and the average accuracy of the model was 0.89. The model can be used to predict and verify the mechanical properties of samples under other saturation and confining pressure conditions in the limited region. The research results can provide theoretical reference for the deterioration mechanism of confining pressure in water-rich roadway.
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