Mixing in extrusion is a vital part of achieving consistent and high-quality extrudates, with residence time being an elucidative measure of the mixing performance. Recent studies around numerical modeling of residence time distributions in single-screw extruders appear to consider flooded extruders mainly. This paper introduces a new and general CFD model to characterize the extruder fill length and residence time distribution for a viscoplastic ceramic material in a starve-fed extruder, including free surface tracking. The CFD model simulates a pulse-injection test, where a fluid parcel is injected at the inlet, with subsequent outlet concentration measured over time. The study includes material characterization and model validation based on laboratory tests. Results quantify the impact of accounting for the partially filled extruder instead of assuming it to be flooded, addressing the potential error when only considering simple analytical approximations to calculate system average residence times. Results further show the ability to fit simulation results to more simple analytical models. This underlines the importance of including the entire extrusion system and forming the basis for further work toward enabling real-time model predictions in starve-fed extrusion systems.

This paper presents a non-isothermal, non-Newtonian Computational Fluid Dynamics (CFD) model for the mixing of a highly viscous polymer suspension in a partially filled sigma blade mixer. The model accounts for viscous heating and the free surface of the suspension. The rheological model is found by calibration with experimental temperature measurements. Subsequently, the model is exploited to study the effect of applying heat both before and during mixing on the suspension’s mixing quality. Two mixing indexes are used to evaluate the mixing condition, namely, the Ica Manas-Zlaczower dispersive index and Kramer’s distributive index. Some fluctuations are observed in the predictions of the dispersive mixing index, which could be associated with the free surface of the suspension, thus indicating that this index might not be ideal for partially filled mixers. The Kramer index results are stable and indicate that the particles in the suspension can be well distributed. Interestingly, the results highlight that the speed at which the suspension becomes well distributed is almost independent of applying heat both before and during the process.