The influence of heat treatment on the microstructure of AISI M2 type high-speed steels modified with powder additions of W and TiB2 was studied. The primary focus was on the effects of austenitizing temperatures on the prior austenite grain size and size distribution, volume fraction, and morphology of the eutectic carbides M2C, M6C, and MC, as well as the character of the secondary precipitation of carbides in the high-speed steels studied. It was shown that austenitizing significantly affects the changes in the chemical composition, morphology, size, and character of distribution of the eutectic carbides in the high-speed steels studied, as well as the volume fraction of retained austenite in the matrix and the prior austenite grain size. These changes in carbides seemed to be induced by a diffusion-induced redistribution of alloying elements between the steel matrix and the carbide phases due to their mutual interaction at high temperatures, which is accompanied by carbide decomposition, coagulation and dissolution and, as a consequence, saturation of the solid solution by alloying elements.
The transformation of the solidification microstructure and the phase changes in AISI M2 grade high-speed steel modified with powder addition of TiB2have been studied focusing on the effect of austenitising temperatures. In order to investigate kinetics of both the microstructure and phase transformations in eutectic carbides, primarily M2C carbide decomposition, upon heat treatments with respect to diffusion processes, different techniques of electron scanning microscopy, X-ray diffraction analysis and energy dispersive X-ray spectrometry have been used.
This paper considers the assessment of attenuation in aluminium alloys castings prepared by gravity casting method and under pressure. The issue of ultrasound attenuation is important in setting the conditions of non-destructive testing, especially in casted materials. The characteristics of the ultrasonic technique, the calculation of the attenuation and the velocity of ultrasound are presented in the theoretical part of this paper. For experimental measurements, cylindrical castings from AlSi alloy were made. The ultrasonic records of the casting control, the calculation of ultrasound attenuation for individual samples as well as the microstructures are listed and described in the experimental part. The evaluation of measurements and comparison of calculated ultrasound attenuation is at the end of this article.
The aim of the article was to check the internal defects in the butt welded joints by non-destructive TOFD (Time of Flight Diffraction) technique. Subsequently, the macrostructure from the defect indication site was evaluated and assigned to the TOFD ultrasound indication. Basic knowledge of ultrasonic TOFD testing are described in the theoretical part of a submitted paper. Ultrasound technique TOFD is non-destructive method that can detect internal defects inside test material without damaging it. It is a reliable method for detecting mainly flat internal defects such as incomplete root penetration, lack of fusion, etc. Ultrasonic test procedures and test results obtained in non-destructive testing of butt weld are shown in experimental part. Evaluation of the ultrasonic TOFD testing results, its advantages and disadvantages are described at the end of this article.
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