Implant surface properties of Ti6Al4V alloy that is currently used as a biocompatible material because of a variety of unique properties can be improved by a self-organized TiO2 layer. The TiO2 nanotubes forming on the titanium-based materials is a relatively recent technology for the surface properties modification and represents pronounced potential in promoting cell adhesion, proliferation, and differentiation that facilitate an implant osseointegration. This work focuses on the influence of surface treatment quality and anodic oxidation parameters on the structure features and properties of TiO2 nanotube coatings. The nanotubes were formed on Ti6Al4V alloy substrates by simultaneous surface oxidation and controlled dissolving of an oxide film in the presence of fluorine ions. The anodization process on ground or polished samples was performed at experimental condition of 30 V for 1 h. The selected anodized samples were heat treated for 2 h at 500 °C under flowing argon. All samples were characterized by scanning electron microscopy, X-ray diffraction analysis, and Raman spectroscopy. The corrosion rate in physiological solution reached 0.0043, 0.0182, and 0.0998 mm per year for the samples in polished and not-anodized, as-anodized, and anodized-heat treated conditions, respectively.

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The study of the effect of thermal treatment conditions on NiTi alloy used in biomedicine was carried out. The experimental samples of NiTi alloy with 55.8 wt% Ni were subjected to the heat treatment. The thermal regimes consisted of aging treatment at 300, 350 and 400 °C for 30 minutes followed by air cooling. The microstructures before and after the heat treatment were observed by optical microscopy. The study was completed by the microhardness measurement and XRD analysis. The obtained results show that the aging temperatures led to microstructural and microhardness changes for the investigated alloy.

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