Nuclear magnetic resonance (NMR)
spectroscopy is a widely used
analytical technique for molecular structure determination, and is
highly valued in the fields of chemistry, biochemistry, and medicinal
chemistry. The importance of NMR methods in the European (PhEur) and
United States Pharmacopeia (USP) is steadily growing. However, undergraduates
often have problems becoming familiar with handling the complex data.
We have developed a simple experiment in which undergraduates, who
are learning 1H NMR spectroscopy for the first time, investigate
natural amino acids, and determine their structure and identity using
low-field 1H NMR measurements and simple COSY experiments.
These students see and learn the connection between the chemical shift
of the αC-proton and the isoelectric point of the amino acid.
They engage with the spectroscopic topic by acquiring their own spectra,
and processing and interpreting the data. Understanding important
natural amino acids and their physicochemical character is highly
relevant to all students studying life sciences.
The monitoring and the control of air pollution which is a consequence of the activities of district heating plants in the area of Niš have indicated that there is a cause and effect relationship between the emitted pollutants and air quality on one hand, and health risk on the other hand. The aim of this paper is to determine the correlation between district heating plants, air quality and health risk. The evidence of this connection is the hazardous health quotient and the level of total carcinogenic risk in comparison to measured immission concentration and expected immission concentrations of pollutants from district heating plants in the city.
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