Pilot plant studies on a sieve tray with %-in. diameter holes and its downcomer were carried out for the systems air/water, air/aqueous glycerol, air-02/water, air-C02/water, air-C02/aqueous sodium carbonate, and air-C02/aqueous caustic soda. Comprehensive experiments on hydraulics, mass transfer, efficiency, and interfacial area were conducted in the same apparatus so that interactions could be studied between the significant parameters. A range of values of gas and liquid rates, at a constant weir height, were studied with respect to (i) hydraulic parameters such as pressure drop, liquid heads, and froth heights on the tray, and (ii) tray efficiency, number of transfer units, and the mass transfer coefficient. Measured values of interfacial area of the froth were obtained for a range of flow rates of the liquid.

Solder Joints are among the most vulnerable components within electronic packages, and solder joint fatigue is regarded to be one of the major methods of electronic package failure. The prediction of solder joint reliability is thus of great importance and most finite element packages utilize the Anand Viscoplastic Model to model the mechanical behavior of the solder joint material. In this work, 3 × 3 arrays of SAC305 solder joints of roughly 750 μm in diameter were reflowed in between two FR-4 printed circuit boards to create a sandwich structural sample. These samples were then subjected to creep testing in shear at various temperatures (T = 25, 50, 75, 100 °C) and stress levels (τ = 5, 10, and 15 MPa). A set of specially designed fixtures was used to grip the solder joint specimens. The nine Anand model constants were then extracted from the creep data. The Anand model predicted creep response curves were then compared with the experimental creep measurements to determine the accuracy of the model. The Anand model predictions were found to match the measured data very well over a wide range of temperatures and stress levels.

In temperature changing environments, solder joints often experience fatigue failure due to cyclic mechanical stresses and strains induced by mismatches in the coefficients of thermal expansion. These stresses and strains lead to damage accumulation and contribute to the crack initiation, crack propagation, and eventually to failure. In this study, we have investigated the cyclic stress-strain behavior of SAC305 and SAC_Q reflowed lead free solders that occur at various testing temperatures and with various prior aging conditions. Lead free solder uniaxial test specimens with circular cross-section have been prepared using vacuum suction method and then were aged for 0 to 20 days at 125 °C. The samples were then subjected to cyclic stress-strain loading using a Micro-mechanical tester at different testing temperatures from T = 25 C to T = 100 C. The evolution of hysteresis loops with duration of prior aging was characterized by measuring the strain energy density dissipated per cycle (loop area), peak stress, and plastic strain range. It was observed that aging degrades the mechanical fatigue properties due to microstructural coarsening. At elevated temperatures, a drop in the loop area and peak stress and an increase in the plastic strain range for both lead free reflowed solder materials were obtained. In addition, SAC_Q samples had a higher loop area and peak stress compared to SAC305.

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