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A well-designed acid stimulation treatment is a rapid well intervention operation that can lead to long-trim economical benefits. In carbonates, the main challenge is to better design acid stimulation treatments in order to meet the two main characteristics of carbonate reservoirs which are high water production and a wide range of heterogeneities. Acid diversion is one of the key factors for a proper distribution of acid which determines the success of these treatments, especially in heterogeneous carbonate formations. In this study, we aim at producing novel solutions in order to reduce water production and enhance zonal coverage through effective diversion. The ultimate goal is to validate a single pumping sequence that combines water mitigation, diversion and acid injection. In order to achieve this, we rely on an integrated R&D approach combining single core and dual core experimental setups. The advantage of the dual core setup is to investigate different permeability contrasts, different saturations configurations and to experimentally validate wormholing in heterogeneous carbonates. In fact, in carbonate effective diversion happens when acid is flowing in the low permeability area at sufficient velocity. An easy way to validate this is through parallel core flooding. We performed a series of high pressure and temperature single and dual core flooding experiments over a range of different carbonate samples having different permeability and porosities. The injection took place at 90 °C and 250 bars. We assessed the efficiency of polymer adsorption by measuring permeability during, before and after polymer injection. Computed Tomography scans were used in order to validate our conclusions. We showed that, adsorption of polymer in carbonates is possible but needs careful design. We experimentally investigated acid diversion in high permeability contrasts (matrix-fissures) through core flooding. This is another novelty in this study. Finally, the combined pumping sequences were experimentally assessed. We validated diversion in carbonates and identified the optimum injection rates required for such applications. An optimum configuration of permeability contrasts and saturations exists for a combined pumping sequence. The experimental results and observations are translated into a series of guidelines and procedures which are directly applicable to acid stimulation field operations. The areas of future required research in applied fluid-rock interactions will be highlighted.