Nanohardness and Effective Elastic Moduli were measured for pulsed-Gas Tungsten Arc Welded Ti-5Al-2.5Sn alloy using autogenous mode through nanoindentation and atomic force microscopy. Experiments were conducted using a Berkovich tip on nanoindentor with Berkovich tip and elliptical pile ups were measured using an Atomic Force Microscope. Nanohardness and effective elastic moduli were calculated in the base metal, heat affected zone and fusion zone of the weldments using different approaches namely Oliver–Pharr method, AFM analysis and work of indentation. A significant difference was observed in the nanomechanical response using these approaches which was attributed to the pile up morphology of the nano indents. The presence of residual stress in the weldments also significantly influenced the nanohardness profile across the weld joint. The present research suggested that the work of indentation is most suitable for assessment of nanomechanical properties of Ti-5Al-2.5Sn alloy weldments among the three techniques studied in this investigation.
Indentation creep was used to analyze the heterogeneity of the mechanical properties in base metal, heat affected zone and fusion zone of titanium alloy weldments obtained using TIG welding process which is generally employed in aerospace industries. For all the weld zones, creep deformation was analyzed using nanoindenter, AFM and microhardness testing. Nanoindentation creep depth was plotted with respect to time using data from the hold stage and CSRs were calculated using empirical relations. The analysis of creep stress exponents (CSE) was indicative of an active creep mechanism for all the weld zones however, a notable variation between the stress exponents and creep mechanism was observed among base metal, heat affected zone and fusion zone. Moreover, Vickers microindentation was used to measure creep of Ti-5Al-2.5Sn alloy weldment using Sargent-Ashby model. However, it did not give the realistic values creep behavior when compared to literature and nanoindentation measurements. It was observed that the phase change, grain size and the loading strain rate (LSR) significantly affected the creep behavior of the Ti-5Al-2.5Sn weldment.
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