Abstract. This paper is devoted the preparation of low cost microfiltration membranes using Moroccan clay powder. The preparation of membrane was composed with two steps: First a macroporous tubular support with a pore diameter 10 µm and porosity 43%. Secondly a microfiltration layer was performed by the slip casting method. A deflocculated slip was obtained by mixing mineral powder of ZrO2, PVA (polyvinyl alcohol) and water, after drying at room temperature for 24 h, the microfiltration layer was heated to 800°C for consolidation. Scanning electron microscopy observation showed homogeneous layers without cracks with an average pore diameter of 0.19 µm for the active layer. Water permeability obtained is about 841 L/h.m2.bar. The membranes have been tested to cleaning of colored wastewater.
In the present study, the effect of Sintering temperature, Particle size and Heating rate of the ceramic support membrane Elaboration based on dry clay were evaluated using full factorial design and investigated by porosity and mechanical strength measures. The flat supports have been prepared from 5 g of the material with a two fraction 2 and 30 µm, the extrusion was performed using the uniaxial pressing in applicant a pressure of 12 tones, the supports sintered between 900° C and 1200°C with a different heating rate (1°C/min and 10°C/min). By using full factorial design 23, it was found that the sintering temperature is the main controlling factors of the physical properties of dry ceramic support membrane, and its increase had a positive effect on Mechanical strength and negative effect on porosity. The interactions between the factors were relatively less important, and they had different (antagonistic/synergetic) influence on the properties. The optimal factors to elaborate the support membrane include a particle size of 2 µm, sintering temperature of 950°C, Heating rate of 1°C predicting the porosity of 40, 8% and Mechanical strength of 12 MPa.
scite is a Brooklyn-based organization that helps researchers better discover and understand research articles through Smart Citations–citations that display the context of the citation and describe whether the article provides supporting or contrasting evidence. scite is used by students and researchers from around the world and is funded in part by the National Science Foundation and the National Institute on Drug Abuse of the National Institutes of Health.