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The extraction part of the technological scheme for radiochemical separation of components of irradiated vanadium-chromium-titanium (V-Cr-Ti) alloy and for their purification from metallic activation products was tested on the whole using activated alloy specimens. It was shown that the replacement of the acid re-extraction of vanadium with a peroxide re-extraction and of the acid re-extraction of chromium with an alkaline re-extraction substantially improves the characteristics of the extraction reprocessing of the activated V-Cr-Ti alloy. In particular, the durations of the vanadium and chromium re-extractions were shortened by about an order of magnitude, the outputs of these alloy components increased, vanadium purification from rare-earth metals became twice as great, and chromium decontamination from cobalt increased by two orders of magnitude.