Honey represents a natural, agricultural product endowed with valuable nutritional and pharmacological functions. Therefore, the classification and evaluation of honey has always been a challenge for chemical analysis, especially when honey adulteration is increasing. The traditional methods for quality control of honey is currently based on physicochemical methods, which is often relatively high cost and time‐consuming. NMR based metabolomics is a metabolomic fingerprinting approach for NMR data using chemometric tools. This combined approach can be apply in food analysis for origin discrimination, biomarker discovery and authenticity screening. The present study demonstrated the capability of the 1H NMR based metabolomics for evaluation of 27 NMR spectra of 09 selected honey samples from Viet Nam. 1H NMR analysis was conducted immediately on collected honey samples, without extraction. Unsupervised PCA multivariate data analysis, applied on 1H NMR experimental data, used to characterize and classify honey samples according to their origin and quality. Different metabolites specific for each botanical origins of honey samples also determined. The obtained results of the demonstration suggests that this combined approach could be useful to develop generally applicable metabolomic approaches to valuate honey products as well as other agricultural products.
High damping rubber (HDR) is used in HDR bearings (HDRBs) which are dissipating devices in structural systems. These devices actually have to support permanent static load in compression and potential cyclic shear when earthquakes occur. Mastering the behavior of bearings implies an accurate understanding of HDR response in such configuration. The behavior of HDR is, however, complex due to the nonlinearity and time dependance of stress-strain response and especially Mullins effect. To the authors' knowledge, tests on HDR under combined quasi-static compression and cyclic shear (QC-CS) have not been performed with regard to Mullins effect yet. The purpose of this study is thus to assess experimentally Mullins effect in HDR, especially under QC-CS. In order to achieve this aim, cyclic tensile and compression tests were first carried out to confirm the occurrence of Mullins effect in the considered HDR. Then, an original biaxial setup allowing testing HDR specimen under QC-CS was developed. This setup enables us to identify Mullins effect of the considered HDR under this kind of loading. Tests carried out with this setup were thus widened to the study of the influence of compression stress on shear response under this loading, especially in terms of shear modulus and density of energy dissipation.
In this paper, the extraction conditions of ulvan from green seaweed Ulva lactuca by using Ultrasound-assisted extraction method were optimised. Experience was designed using Box-behnken model with experient areas as following: extraction temperature (X1: 50–90 °C), extraction time (X2: 20–40, min) and solvent-to-material ratio (X3: 50/1–70/1, v/w), objective function (Y: extraction yield) was required to get maximum value. The result showed that the optimization conditions for extraction were: extraction temperature 84.28 °C, extraction time 30.59 min with 60.21/1 (v/w) as solvent-to-material ratio, and the expected objective function Y is 22.86% based on dried seaweed weight.
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