The transition in the use of fiber composite structures from special applications to application in the mass market is accompanied by high demands in quality assurance. The consequential costs of unclear process design, unknown fiber orientations, and uncertainty regarding the effects of any fiber angle deviations can lead to market considerations (higher costs/time for development) in mass production that advise against the use of fiber composites, despite their superiority compared with conservative materials. Active monitoring of the deposited reinforcement layers and an evaluation of the real fiber orientation can form the basis of a robust industrial use of fiber composites by a first-time right production that is able to reduce the process variability. This paper describes the application of an image analysis system to provide both geometric topology and local reinforcement fiber orientation feedback to a finite-element (FE) model. The application during an industrial composite part production is described, and the possibilities of using it for the improvement of the lightweight character, the reduction of rejects, and the realization of a quality management system are shown. The determined component data are made directly available for use in numerical simulations and, thus, they serve as a non-destructive evaluation of the components under real conditions in which all production-dependent influences that affect the fiber orientation are incorporated.

A cure kinetics investigation of a high temperature-resistant phenol novolac cyanate ester toughened with polyether sulfone (CE-PES blend) was undertaken using non-isothermal differential scanning calorimetry. Thin ply carbon fiber prepreg, based on the CE-PES formulation, was fabricated, and plates for further in-situ cure monitoring were manufactured using automated fiber placement. Online monitoring of the curing behavior utilizing Optimold sensors and Online Resin State software from Synthesites was carried out. The estimation of the glass transition temperature and degree of cure allowed us to compare real time data with the calculated parameters of the CE-PES formulation. Alongside a good agreement between the observed online data and predicted model, the excellent performance of the developed sensors at temperatures above 260 °C was also demonstrated.

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The objective of this study is to describe the stress relaxation behavior of an epoxy-based fiber-reinforced material. An existing incremental formulation of an orthotropic linear viscoelastic material behavior was adapted to Voigt notation and to the special case of an isotropic material. Virtual relaxation tests on a representative volume element were performed, and the behavior of individual components of the relaxation tensor of the transversely isotropic composite material was determined. The study demonstrated that in the case of only one viscoelastic material, each component of the relaxation tensor can be described in terms of a scalar form factor and the behavior of the neat resin. The developed method was implemented in an incremental finite element model (FEM) analysis to calculate the stress relaxation on the macroscopic ply level. A validation of the approach has shown a promising agreement up to a limit below the glass transition temperature of 15 °C in longitudinal and 35 °C in transverse direction. This study therefore demonstrates a novel way to incrementally describe the macroscopic viscoelastic behavior of materials with a single viscoelastic component with good controllability for engineering purposes.

The objectives of this study were to experimentally determine the effects of the stress relaxation of a cyanate-ester-based composite, derive and integrate constitutive equations into commercial FEM software, and apply this approach to understand the formation of residual stress in a typical aerospace structure—namely, a stiffened panel. In preliminary studies, a cyanate-ester-based composite with increased fracture toughness for high-temperature applications was developed. High curing temperatures up to 260 °C will inevitably lead to high process-induced stresses. To assess the magnitude of impact on the development of internal stresses, the relaxation behavior of the neat resin was measured and characterized. The system was toughened, and the effect of stress relaxation increased as the temperature got closer to the glass transition temperature of the toughener, which was approximately 240 °C. With the use of an incremental linear viscoelastic model, the relaxation behavior was integrated into a process model with a holistic approach. A stiffened panel was manufactured and used as the validation use case. The displacement field was validated with an optical 3D measuring system, and good agreement was found between the simulated and experimental results. The maximum difference between the elastic and the viscoelastic solution was found to be 15%. Furthermore, the stress magnitude in the transverse material direction resulted in a more critical value higher than the material strength.