We have obtained an excitation of longitudinal bulk acoustic waves in a diamond-based High overtone Bulk Acoustic Resonator (HBAR) at microwave and enhanced frequency bands as EHF up to 40 GHz. As an effective piezoelectric transducer, an aluminum-scandium nitride film is employed. The frequency response of acoustic overtones excited in the HBARs with a different aperture in the 1.0 up to 40 GHz range is measured. Some peculiarities of HBAR's frequency response concerned with the thin film piezoelectric transducer are studied. It is established that the maximal magnitude of the quality factor varies near the value of about 10 000 within all the frequency bands investigated. The approximately frequency-independent Q-factor behavior can explain in terms the Landau–Rumer approximation describing the acoustic attenuation in a diamond. An estimation of the HBAR's quality parameter as Q × f ≈ 4 × 1014 Hz at 40 GHz is obtained. In our opinion, that value exceeds all known data among the given devices. The results obtained will be helpful in the development of microwave and EHF acoustic resonators as well as highly sensitive acoustic sensors. The development of the EHF band opens up the possibility of obtaining acoustic waves of submicrometer and nanometer scales (in various media) and implementing acoustic studies of micro- and nanoobjects.

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New theoretical and experimental results of microwave acoustic wave propagation in diamond-based multilayer piezoelectric structures (MPS) as “Me1/(Al,Sc)N/Me2/(100) diamond/Me3” and “Me1/AlN/Me2/(100) diamond/Me3” under three metal film depositions, including the change in the quality factor Q as a result of Me3 impact, were obtained. Further development of our earlier studies was motivated by the necessity of creating a sensor model based on the above fifth layered MPS and its in-depth study using the finite element method (FEM). Experimental results on the change in operational checkpoint frequencies and quality factors under the effect of film deposition are in satisfactory accordance with FEM data. The relatively small decrease in the quality factor of diamond-based high overtone bulk acoustic resonator (HBAR) under the metal layer effect observed in a wide microwave band could be qualified as an important result. Changes in operational resonant frequencies vs. film thickness were found to have sufficient distinctions. This fact can be quite explained in terms of the difference between acoustic impedances of diamond and deposited metal films.