The existing mold concept of fabricating magnetorheological elastomer (MRE) tends to encounter several flux issues due to magnetic flux losses inside the chamber. Therefore, this paper presents a new approach for enhancing particle alignment through MRE fabrication as a means to provide better rheological properties. A closed-loop mold, which is essentially a fully guided magnetic field inside the chamber, was designed in order to strengthen the magnetic flux during the curing process with the help of silicone oil (SO) plasticizers. The oil serves the purpose of softening the matrix. Scanning electron microscopy (SEM) was used to observe the surface morphology of the fabricated MRE samples. The field-dependent dynamic properties of the MREs were measured several ways using a rheometer, namely, strain sweep, frequency sweep, and magnetic field sweep. The analysis implied that the effectiveness of the MRE was associated with the use of the SO, and the closed-loop mold helped enhance the absolute modulus up to 0.8 MPa. The relative magnetorheological (MR) effects exhibited high values up to 646%. The high modulus properties offered by the MRE with SO are believed to be potentially useful in industry applications, particularly as vibration absorbers, which require a high range of stiffness.
In this study, three types of available processing aids; namely naphthenic oil (PTO), light mineral oil (MO) and epoxidised palm oil (EPO), were used as a dispersing agent to investigate the effects of physicochemical and viscoelastic properties of magnetorheological elastomers (MREs). EPO was selected as the natural-based processing aids, and its morphological, magnetic properties, mechanical and rheological properties of EPO based MREs was compared with the petroleum-based dispersing aids such as light MO and PTO at a fixed amount of 10 phr. The results indicated that EPO was the best alternative of dispersing agent for the MRE rather than the light MO and PTO. In addition, the morphological, magnetic and mechanical properties of the MRE suggested that the EPO could promote compatibility and provide a better lubricant property between the rubber molecular and magnetic particles. It has been observed that the field-dependent storage modulus and MR effect of MRE samples were improved with the addition of dispersing aids, where the MR effect of MRE with the EPO has showed the highest performance of 12%.
Cobalt particles have been introduced as a filler due to the advantages of embedding their magnetic and electrical properties in magnetorheological elastomer (MRE). In the present research, the rheology and resistance of MRE are experimentally evaluated. Isotropic and anisotropic MRE samples containing silicone rubber and cobalt particles were fabricated. The magnetic properties of MRE are conducted using a vibrating sample magnetometer (VSM). The morphological aspects of MRE are observed by using field emission scanning electron microscopy (FESEM) and characterized by energy-dispersive X-ray spectroscopy (EDX). Rheological properties under various magnetic field strengths were measured for the magnetic field, strain amplitude, and frequency sweep test by using a parallel-plate rheometer. Subsequently, the resistance of MRE is tested under different applied forces and magnetic fields. The MRE storage modulus depicted an enhancement in field-dependent modulus across all the applied magnetic fields. The electrical resistance generated from the sample can be manipulated by external magnetic fields and mechanical loads. The conductivity of MRE is due to the existence of cobalt arrangements observed by FESEM. By introducing cobalt as filler and obtaining satisfactory results, the study might open new avenues for cobalt to be used as filler in MRE fabrication for future sensing applications.
This paper investigates the field-dependent rheological properties of magnetorheological (MR) fluid used to fill in MR dampers after long-term cyclic operation. For testing purposes, a meandering MR valve was customized to create a double-ended MR damper in which MR fluid flowed inside the valve due to the magnetic flux density. The test was conducted for 170,000 cycles using a fatigue dynamic testing machine which has 20 mm of stroke length and 0.4 Hz of frequency. Firstly, the damping force was investigated as the number of operating cycles increased. Secondly, the change in viscosity of the MR fluid was identified as in-use thickening (IUT). Finally, the morphological observation of MR particles was undertaken before and after the long-term operation. From these tests, it was demonstrated that the damping force increased as the number of operating cycles increases, both when the damper is turn on (on-state) and off (off-state). It is also observed that the particle size and shape changed due to the long operation, showing irregular particles.
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