The objective of this study was to determine the effect of selected surface treatments on the surface texture of a feldspathic porcelain. The three different etchant treatments were, acidulated phosphate fluoride (APF) applied for 10 min and hydrofluoric acid (HF) applied for 1 and 4 min. After acid treatment, half of the specimens from each group were cleansed with water and others were subjected to ultrasonic cleaning and then dried. Half of the specimens cleansed with two different methods were treated with silane. Scanning electron microscopy (SEM) and energy dispersive spectroscopy (EDS) were used to characterize the effects of such treatments. Etching with APF displays shallow patterns. Etching for 1 min with HF displays deep channels, pores and precipitates on the surface and as the etching time increased these channels were replaced by larger channels. EDS analyses show that the crystalline precipitates on the etched surfaces, which were not readily soluble in water, were the reaction products of Na, K, Ca, Al, etc. HF displayed a more roughened surface than the APF gel. However, the precipitates remain on the surface after acid application, they can only be removed by ultrasonic cleaning and cannot be removed by rinsing.
The aim of this study was to measure the colour stability and viscoelastic properties of three commercially available soft lining materials in vitro, by exposing them to 3% erythrosine, tartrazine and sunset yellow solutions. The colour changes were determined using a computer controlled spectrophotometer. The colour change of three soft lining materials--Molloplast B, Flexor and Coe Super Soft--were determined after 1, 3 and 6 months storage in three different food colorant solutions. The colour changes of Molloplast B was not noticeable. Only the initial colour value of Flexor was significantly different from the other time interval colour measurements. On the other hand, the colour difference of Coe Super Soft was found to be significantly different at all comparative time interval measurements (P<0.05). According to Shore A hardness values, Molloplast B had an initial hardness of 44 in all three solutions, and there was a slight increase after 6 months. Flexor had an initial hardness of 39, at the end of 6 months the hardness changed a little. Coe Super Soft was fairly hard after processing and Shore A hardness was initially 89 which increased to 95 later on. According to these results, only the hardness values of Coe Super Soft showed a statistically significant difference when compared using Wilcoxon signed rank test at the P<0.05 level. As a conclusion, silicon type soft lining material seems to be more resistant to colour change and hardness than the acrylic type soft liners.
Fracture strength of denture base resins is of great concern, and many approaches have been used to strengthen acrylic resin dentures. Fracture resistance of six commercially available acrylic resin denture base materials were compared, through impact and transverse strength tests. Three rapid heat-polymerised resins (QC 20, Meliodent and Trevalon), two high-impact strength resins (Trevalon Hi and Lucitone 199) and a strengthened injection-moulded acrylic resin (SR Ivocap plus) were included in the study. Twenty acrylic resin test specimens were fabricated from each resin. For impact strength test, ten notched specimens were tested in a Charpy-type impact tester. The other ten specimens were used for transverse strength tests, deflection and modulus of elasticity values were also determined, which were assessed with three-point bending tests using an Universal Testing Machine. Impact test values showed significant differences among acrylic resins (F= 4.817 p = 0.0). SR Ivocap resin showed the highest impact strength values, followed by Trevalon Hi and Lucitone 199. The transverse strength test values were not significant when six acrylic resins were compared (F= 1.705 p = 0.151). High-impact resins can be recommended to increase the impact strength of denture base. If the cause of fracture is mechanical or anatomical, strengthened acrylic resins and conventional acrylic resins have similar fracture resistance.
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