Geopolymer concrete has the potential to replace ordinary Portland cement which can reduce carbon dioxide emission to the environment. The addition of different amounts of steel fibers, as well as different types of end-shape fibers, could alter the performance of geopolymer concrete. The source of aluminosilicate (fly ash) used in the production of geopolymer concrete may lead to a different result. This study focuses on the comparison between Malaysian fly ash geopolymer concrete with the addition of hooked steel fibers and geopolymer concrete with the addition of straight-end steel fibers to the physical and mechanical properties. Malaysian fly ash was first characterized by x-ray fluorescence (XRF) to identify the chemical composition. The sample of steel fiber reinforced geopolymer concrete was produced by mixing fly ash, alkali activators, aggregates, and specific amounts of hook or straight steel fibers. The steel fibers addition for both types of fibers are 0%, 0.5%, 1.0%, 1.5%, and 2.0% by volume percentage. The samples were cured at room temperature. The physical properties (slump, density, and water absorption) of reinforced geopolymer concrete were studied. Meanwhile, a mechanical performance which is compressive, as well as the flexural strength was studied. The results show that the pattern in physical properties of geopolymer concrete for both types of fibers addition is almost similar where the slump is decreased with density and water absorption is increased with the increasing amount of fibers addition. However, the addition of hook steel fiber to the geopolymer concrete produced a lower slump than the addition of straight steel fibers. Meanwhile, the addition of hook steel fiber to the geopolymer concrete shows a higher density and water absorption compared to the sample with the addition of straight steel fibers. However, the difference is not significant. Besides, samples with the addition of hook steel fibers give better performance for compressive and flexural strength compared to the samples with the addition of straight steel fibers where the highest is at 1.0% of fibers addition.
Geopolymerization consists of several chemical reactions that has been reported widely as an exothermic reaction. Previous studies on heat released during geopolymerization used metakaolin and fly ash of F class as a precursor for geopolymer. Meanwhile, in this study, fly ash of C class is used and a preliminary study has been conducted on determining the exothermic reaction of the geopolymerization with various ratios of solid-to-liquid ranging from 1.5 to 2.5. The amount of heat released was determined by using Differential Scanning Calorimeter. It was proven that different solid-to-liquid ratio affected the amount of heat released during geopolymerization as the highest amount of the heat released were recorded at the optimum solid-to-liquid ratio of 2.0.
Geopolymers have been intensively explored over the past several decades and considered as green materials and may be synthesised from natural sources and wastes. Global attention has been generated by the use of kaolin and calcined kaolin in the production of ceramics, green cement, and concrete for the construction industry and composite materials. The previous findings on ceramic geopolymer mix design and factors affecting their suitability as green ceramics are reviewed. It has been found that kaolin offers significant benefit for ceramic geopolymer applications, including excellent chemical resistance, good mechanical properties, and good thermal properties that allow it to sinter at a low temperature, 200 °C. The review showed that ceramic geopolymers can be made from kaolin with a low calcination temperature that have similar properties to those made from high calcined temperature. However, the choice of alkali activator and chemical composition should be carefully investigated, especially under normal curing conditions, 27 °C. A comprehensive review of the properties of kaolin ceramic geopolymers is also presented, including compressive strength, chemical composition, morphological, and phase analysis. This review also highlights recent findings on the range of sintering temperature in the ceramic geopolymer field which should be performed between 600 °C and 1200 °C. A brief understanding of kaolin geopolymers with a few types of reinforcement towards property enhancement were covered. To improve toughness, the role of zirconia was highlighted. The addition of zirconia between 10% and 40% in geopolymer materials promises better properties and the mechanism reaction is presented. Findings from the review should be used to identify potential strategies that could develop the performance of the kaolin ceramic geopolymers industry in the electronics industry, cement, and biomedical materials.
The present work studies the effect of solid-to-liquid (S/L) ratio on the properties of thin fly ash-based geopolymer. The fly ash geopolymers with dimension of 160 mm × 40 mm × 10 mm were synthesised by using various S/L ratios (1.5, 2.0, 2.5, 3.0 and 3.2). The alkali activator was prepared by mixing 10M sodium hydroxide (NaOH) solution and sodium silicate (Na2SiO3) with the Na2SiO3/NaOH ratio of 2.5. The samples were cured at 60°C for 6 hours. The performance of fly ash geopolymers was evaluated by testing the flexural strength after 28 days. Results showed that the S/L ratio had an effect on flexural strength. The optimum flexural strength of 5.12 MPa was achieved by the fly ash geopolymer with S/L ratio of 2.5. However, the flexural strength dropped with higher S/L ratio as the workability decreases. However, further experimental lab work should be carried out as there is less knowledge in the study on the flexural strength of thin fly ash geopolymer.
Nowadays, the consumption of lead-free solder has been widely used around the world since the utilization of SnPb solder has been banned and restricted by European Union. Variety of studies have been conducted by the researchers to find an alternative to replace the usage of SnPb such as SnCu, SAC, SnAg and etc. However, the development of plain lead-free solder was declared to provide low mechanical, thermal, and electrical properties in terms of interfacial intermetallic compound and wettability towards its solder joint compare to the traditionally monolithic SnPb solder alloy. Mostly, previous studies stated that addition of some additives such as ceramic particles (Si 3 N 4, TiO 2, SiC, NiO and etc) may improves the solder joint reliability. At the same time, no major studies were done using geopolymer ceramic as reinforcing agent in plain matrix alloy. Therefore, this paper reviews the fabrication process of multiple geopolymer-based ceramic such as fly ash, kaolin, and slag as reinforcement in solder alloy. The development process includes the processing method of geopolymer ceramic and the characterization of geopolymer ceramic as reinforcing material consist of; i) chemical composition, and ii) phase identification.
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