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Hard magnetic nanopowders of the Nd15Fe78B7 alloy were synthesized by the reduction-diffusion reaction of a stoichiometric mixture of Nd, Fe, and Fe-B oxides with CaH2 in a hydrogen atmosphere at 800 ° C. Nd, Fe, Fe-B oxides were obtained by precipitation and had the form of granules with an average particle size of neodymium oxide - 50 nm, iron oxide - 95 nm, iron borate - 57 nm. The particle size of the Nd15Fe78B7 alloy was 45-140 nm. It is shown that the proposed method is suitable for obtaining nanopowders of hard magnetic alloys of the Nd-Fe-B system.

Hard magnetic nanopowders of the Nd15Fe78B7 alloy were synthesized from mixtures of Nd, Fe and Fe-B oxides with CaH2 in a hydrogen atmosphere at 800 °C by a reduction-diffusion process. Nd, Fe, Fe-B oxides were synthesized by chemical deposition. The resulting particles had a granular shape with an average size: Nd2O3 — 50 nm, Fe2O3 — 95 nm, Fe3BO6 — 57 nm. The particle size of the Nd15Fe78B7 alloy was 45–140 nm. It is shown that the proposed method is suitable for obtaining nanopowders of hard magnetic alloys of the Nd-Fe-B system.

Nanoparticles of the alloy with the composition Nd-Fe-B were formed by the chemical method of co-precipitation reduction using a reducing agent sodium borohydride. The nanoparticle size was 35–95 nm. The silica coating was applied after stabilizing the nanoparticles with APTMS. The core of Nd-Fe-B alloy nanoparticles covered with a SiO2 shell, Nd2Fe14BаSiO2, the particle size was 35–125 nm with a shell width of 8–15 nm.

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