Two crystals with precise parabolic holes were used to demonstrate sagittal beam collimation by means of a diffractive-refractive double-crystal monochromator. A new approach is introduced and beam collimation is demonstrated. Two Si(333) crystals with an asymmetry angle of α = 15° were prepared and arranged in a dispersive position (+,-,-,+). Based on theoretical calculations, this double-crystal set-up should provide tunable beam collimation within an energy range of 6.3-18.8 keV (Θ(B) = 71-18.4°). An experiment study was performed on BM05 at ESRF. Using 8.97 keV energy, the beam profile at various distances was measured. The experimental results are in good agreement with theoretical predictions. Owing to insufficient harmonic suppression, the collimated (333) beam was overlapped by horizontally diverging (444) and (555) beams.

A total beam compression of 5 and 10 corresponding to the asymmetry angles of 9° and 12° is achieved with V-5 and V-10 monochromators, respectively, in standard single crystal pure germanium (220) X-ray beam compressing (V-shaped) monochromators for CuKα 1 radiation. A higher 1D compression of X-ray beam is possible using larger angles of asymmetry, however it is achieved at the expense of the total intensity, which is decreased due to the refraction effect. To increase the monochromator intensity, several ways are considered both theoretically and experimentally. Linearly graded germanium rich Ge x Si (1-x) single crystal was used to prepare a V-21 single crystal monochromator with 15° asymmetry angles (compression factor of 21). Its temperature gradient version is discussed for CuKα 1 radiation. X-ray diffraction measurements on the graded GeSi monochromator showed more than 3-times higher intensity at the output compared with that of a pure Ge monochromator.

Fabry-Perot type multi-plate crystal cavities consisting of compound refractive lenses were prepared on silicon wafers by micro-electronic lithographic techniques. The crystal orientation of this X-ray optical device is the same as that of the two-plate x-ray resonators reported (Phys. Rev. Lett. 94, 174801, 2005). Experimentally, X-ray (12 4 0) back diffraction from these monolithic silicon crystal devices for various photon energies showed interference fringes as a function of photon energy due to cavity resonance, but with less pronounced amplitudes. The expected focusing effect from the CRL is observed and energy-dependent focal length is detected. Detailed analysis on cavity interference and beam focusing will be discussed.Beam shape conditioning and high-resolution monochromatization for laboratory and synchrotron sources is achieved by crystal monochromators with flat surfaces. In coplanar geometries, Bragg reflection geometry is used for single flat diffractors, double diffractor arrangements and Bartels monochromators working in parallel beam set-up. On the other hand, diffractive-refractive optical devices involve non-coplanar geometry arrangement. Devices with V-shape arrangement of flat diffractors or with cylindrical or parabolic grooves set in Bragg non-coplanar geometry focus the incident beam into a distant focal spot. Their focusing properties and their aberrations were studied in the past. Recently, we have extended studies of the diffractive-refractive devices into the Laue geometry. Then both the transmitted and the diffracted beams pass through the device. Therefore, these devices can be prepared as a flat thin plate or as a shaped plate-parabolic, double-parabolic or doubletunnel crystals. Theoretical predictions and the first experiments by synchrotron radiation show focusing properties as well. We will present results of the beam propagation and focusing properties resulting from aligning a sequence of these devices with crystal diffractors with high asymmetry.In this work the effect of complete transfer (from diffractedtransmitted direction to the diffracted-reflected direction) of x-rays for the media with different thermal conductivity is considered in presence of temperature gradient (TG). The media with different conductivities were experimentally realized by simply changing the pressure of the same medium. It has been found experimentally in a quartz monocrystal that the relative intensity of the beam depending from the TG is increasing and at the certain values is saturating. It is seen that with decreasing the pressure from 760 Torr until 10 Torr, decreasing also the corresponding to the complete transfer the magnitude of the TG. The consequent decreasing of the pressure results to increasing the magnitude of the corresponding TG. No saturation is taking place at the smallest pressure (0.03 Torr). We have to mention that for the transmitted beam taking place the contrary scenario. With the increasing the TG the intensity of the beam is decreasing practically until the zero. In orde...