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Al 2 O 3 /xZrO 2 (where x = 0, 3, 13, and 20 wt.%) composite coatings were deposited onto mild steel substrates by atmospheric plasma spraying of mixed a-Al 2 O 3 and nano-sized monoclinic-ZrO 2 powders. Microstructural investigation showed that the coatings comprised well-separated Al 2 O 3 and ZrO 2 lamellae, pores, and partially molten particles. The coating comprised mainly of metastable c-Al 2 O 3 and tetragonal-ZrO 2 with trace of original a-Al 2 O 3 and monoclinic-ZrO 2 phases. The effect of ZrO 2 addition on the properties of coatings were investigated in terms of microhardness, fracture toughness, and wear behavior. It was found that ZrO 2 improved the fracture toughness, reduced friction coefficient, and wear rate of the coatings.