This study contributes to the understanding of the mechanism behind thermo chemical aspects related to the resin transfer moulding manufacturing process of a composite part. The aim is to comprehend the phenomena, to identify related parameters and to get knowledge-based methods for the process development. Therefore, the first part of this study is an experimental study about the behaviour of material properties during the manufacturing process of the single component and the composite. It concludes with constitutive equations for single-process parameters and their associated homogenisation approach for the composite properties. During the manufacturing process, material values of the matrix are changing and influenced by a high number of effects. In the second part, a simulation strategy is been derived. This developed material model integrates a dependency of the time–temperature–polymerisation and fibre volume content. The model is validated in a test case of a manufacturing process of an aircraft component, a fuselage frame.

In this study, the influence of soft substrate surface finishing (5 distinct conditions) on tribological properties of hydrogenated amorphous carbon (a-C:H) films is investigated. Low carbon steel substrates were plasma-nitrided and DLCcoated in a single PECVD batch. Topographical evolution was investigated through white light interferometry (WLI) and scanning electron microscopy (SEM). The substrate topography leads to a negligible impact on bonding structure and mechanical properties of a-C:H films, which were analyzed by Raman spectroscopy (RS) and nano-indentation. The nitriding and deposition process resulted in two groups of samples regarding the topographic features: (A) RoughS q coated & 0.17-0.23 lm; (B) SmoothS q coated & 0.08-0.11 lm. Tribological performance of multifunctional coatings under incremental normal load reciprocating dry sliding tests in ambient air revealed friction coefficients of 0.09 (Rough) and 0.05 (Smooth). Wear scars were analyzed by WLI, SEM and RS. The results suggest that rougher substrates inhibit tribolayer formation and stability, leading to higher friction coefficients.

The adhesion of multifunctional coatings on soft substrates is of paramount importance in the tribological behavior of this important class of surface treatment. In particular, scratch and indentation tests have been extensively used in order to assess this property. In this paper, the adhesion of a-C:H diamond-like carbon films deposited on nitrided low carbon steel was evaluated by indentation and scratch tests. The coatings were produced by PECVD onto 1020 steel substrates with two different surface finishing: ground (Sq = 0.184 µm) and polished (Sq = 0.002 µm). Indentation tests using a Rockwell diamond indenter were conducted and the adhesion evaluated by measuring the spalling region on images obtained by using optical microscopy. The analysis of the spalling regions produced semi-quantitative results, eliminating the subjective qualitative analysis proposed by the standard method VDI 3198. In addition, scratch tests were performed using the same indenter and a comparison between the two techniques was established.

ResumoA adesão de revestimentos multifuncionais em substratos moles é de extrema importância para o comportamento tribológico desta importante classe de tratamentos superficiais. Mais especificamente, testes de indentação e de riscamento são bastante utilizados na medição desta propriedade. No presente estudo, a adesão de filmes de DLC do tipo a-C:H depositados em aço baixo carbono nitretado foi investigada através de testes de indentação e riscamento. Os revestimentos foram produzidos através de PECVD em substratos de aço 1020 com dois acabamentos superficiais: lixado (Sq = 0,184 µm) e polido (Sq = 0,002 µm). Foram realizados testes de indentação Rockwell C e a adesão foi quantificada através da medição da área desplacada em imagens obtidas através de microscopia ótica. Esta análise produziu resultados semi-quantitativos, eliminando a análise qualitativa subjetiva sugerida pela norma VDI3198. Ainda, testes de riscamento foram realizados nas mesmas amostras com o mesmo indentador para que uma comparação entre ambas as técnicas pudesse ser estabelecida. Por fim, o método apresentado mostrou resultados coerentes, onde amostras com menor carga crítica apresentaram uma maior área desplacada. Amostras lixadas apresentaram um desempenho inferior em relação a adesividade. Palavras-chave: Diamond-like carbon; Adesão; Topografia; Aço nitretado. ASSESSMENT OF MULTIFUNCTIONAL COATING ADHESION: COMPARISON BETWEEN INDENTATION AND SCRATCH TESTS AbstractThe adhesion of multifunctional coatings on soft substrates is of paramount importance in the tribological behavior of this important class of surface treatment. In particular, scratch and indentation tests have been extensively used in order to assess this property. In this paper, the adhesion of a-C:H diamond-like carbon films deposited on nitrided low carbon steel was evaluated by indentation and scratch tests. The coatings were produced by PECVD onto 1020 steel substrates with two different surface finishing: ground (Sq = 0.184 µm) and polished (Sq = 0.002 µm). Indentation tests using a Rockwell diamond indenter were conducted and the adhesion evaluated by measuring the spalling region on images obtained by using optical microscopy. The analysis of the spalling regions produced semi-quantitative results, eliminating the subjective qualitative analysis proposed by the standard method VDI 3198. In addition, scratch tests were performed using the same indenter and a comparison between the two techniques was established. Finally, the method presented coherent results, where films with higher critical loads presented lower spalled areas. Ground samples presented an overall poorer adhesion performance.