Abstract NH4SbS2 has been prepared and its crystal structure determined. The new compound crystallizes triclinic, space group P1̄, with the following cell-constants: a = 1213 pm, b = 641.9 pm, c = 634.0 pm, a = 102.9°, β = 98.9°, γ = 101.2°. In the structure there are ψ-SbS4-trigonal bipyramids connected to chains by common edges.
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