In this work, we perform high accuracy measurements of thermophysical properties for the National Institute of Standards and Technology standard reference material for 316L stainless steel. As these properties can be sensitive to small changes in elemental composition even within the allowed tolerances for an alloy class, by selecting a publicly available standard reference material for study our results are particularly useful for the validation of multiphysics models of industrial metal processes. An ohmic pulse-heating system was used to directly measure the electrical resistivity, enthalpy, density, and thermal expansion as functions of temperature. This apparatus applies high current pulses to heat wire-shaped samples from room temperature to metal vaporization. The great advantage of this particular pulse-heating apparatus is the very short experimental duration of 50 ls, which is faster than the collapse of the liquid wire due to gravitational forces, as well as that it prevents any chemical reactions of the hot liquid metal with its surroundings. Additionally, a differential scanning calorimeter was used to measure specific heat capacity from room temperature to around 1400 K. All data are accompanied by uncertainties according to the guide to the expression of uncertainty in measurement. Jeffrey W. Sowards: Formerly with NIST.
NIST SRM 1155a is an AISI 316L stainless steel (Cr18–Ni12–Mo2) and Standard Reference Material (SRM) intended for use with test methods for elemental analysis. In a previous paper “Measurement of thermophysical properties of solid and liquid NIST SRM 316L stainless steel”, we already published reliable thermophysical properties of high temperature solid and of the liquid phase of this material such as temperature dependent enthalpy, density and electrical resistivity, as well as specific heat capacity for the solid and the liquid phase. In this paper, we add additional thermophysical properties obtained by ohmic pulse-heating and by the laser flash method, namely thermal conductivity and thermal diffusivity as a function of temperature. Furthermore we report surface tension measurement results of liquid SRM 1155a obtained by means of electromagnetic levitation. Simulation of processes like additive manufacturing, laser welding, laser cutting or metal casting depend on the above named quantities as input data. Ohmic pulse-heating as well as electromagnetic levitation are so called “containerless” investigation techniques and no significant chemical reactions of the hot liquid alloy with its surrounding occur. The data presented here are compared to the available literature data and are accompanied by an uncertainty analysis according to the “Guide to the Expression of Uncertainty in Measurement”.
In this work, we present normal spectral emissivity data of solid and liquid molybdenum at a wavelength of 684.5 nm. The presented results are novel measurements on molybdenum, a material, which was already measured 15 years ago by our group. The present results indicate a lower emissivity in the liquid phase. The novel measurements were done within the European Metrology Programme for Innovation and Research (EMPIR) project 17IND11 Hi-TRACE. The optimized measuring system is an ohmic pulse-heating apparatus combined with microsecond Division of Amplitude polarimetry.
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