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Lead titanate powders were synthesized via sol-gel combustion method. Citric acid was used as the fuel to reduce the crystallization temperature. The ratios of sol to fuel contents were 1:1 to 1:4 by%w/w. The synthesized powder was characterized by XRD and SEM. The XRD results indicated that the single tetragonal phase can be obtained at the low calcinations temperature (300 • C) with using the ratio of 1:4. The particle are almost spherical shape and the particle size were increased with the increasing of calcinations temperatures and the particle size were about 98-116 nm.