The microstructure, mechanical properties and creep behavior of Mg-Gd-Y-Zr alloys at different temperatures and stresses have been investigated. Results show that the tensile properties and creep resistance at T6 condition is much higher than that at as-cast condition. The creep resistance of Mg-Gd-Y-Zr alloy at 250°C/80MPa is markedly better than that at 300°C/50MPa, indicating that temperature makes more effects on the creep resistance than the stress.
The production of primary aluminum is an energy costly process. With the global warming being of concern, the secondary aluminum stream is becoming an even more important component of aluminum production and is attractive due to its economic and environmental benefits. Recycling of aluminum by new solid state recycling techniques instead of conventional remelting and subsequent refining processing can result in significant energy savings. Severe Plastic Deformation (SPD) techniques have been applied for consolidating nano particles into fully dense materials with good mechanical properties. However, solid state recycling of scraps by SPD is only in the beginning. In the present study, degreasing of aluminum chips from the machine workshop was investigated by a thermal method and chemical treatment. Thereafter, the decoated chips were recycled by Cyclic Extrusion Compression (CEC) at deformation temperatures between 400 and 500 °C. The microstructure and mechanical properties of the recycled aluminum scrap processed by SPD were subsequently investigated. The results show that SPD technology provides a promising alternative for recycling of aluminum scrap. Thermal degreasing of aluminum scrap resulted in more oxidization of aluminum scrap particles. Visible interfaces between chips were observed even at a low magnification.
This paper investigates the microstructure, mechanical properties and creep behavior of Mg–Al–Ca alloys with different Ca content. SEM and EDAX analyses show that the dominant second phase in the as-cast Mg–Al–Ca alloys is Al2Ca, which distributes at the grain boundaries and disperses in the grain interior as well. Both the elevated tensile strength and the creep resistance of Mg–Al–Ca alloys obviously increased with increasing Ca at high temperature. TEM analyses reveal that finer Al2Ca particles with an average size of 0.02 µm precipitated dynamically during the creep process. Selected area electron diffraction (SAD) patterns show that the dynamic Al2Ca precipitates have a coherent interface with matrix as (0110) Mg // (220) Al2Ca, [2110] Mg // [112] Al2Ca. The strengthening mechanism of Mg–Al–Ca alloys at elevated temperature was discussed.
Experiments were conducted both to evaluate the potential for grain refinement, the subsequent mechanical properties at room temperature in samples of AZ31 Mg alloy and also to investigate the relationship between one-step and two-step high ratio extrusion (HRE). The one-step HRE was undertaken using a high extrusion ratio of 70:1 at 250, 300 and 350°C. And the two-step HRE was conducted with an extrusion ratio of 7 for the first step at 250, 300 and 350°C, followed by a second-step extrusion with an extrusion ratio of 10 at 250, 300 and 350°C. The initial grain size in the AZ31 ingot was 100μm and that after one-step HRE became similar to 5μm, after two-step HRE at 250, 300 and 350°C were 2, 4, 7μm, respectively, resulting in superior mechanical properties at ambient temperature. The microstructure of two-step HRE was finer and uniformer than that of one-step HRE and the strength of one-step and two-step HRE were similar, moreover, the elongation of one-step HRE was improved markedly than that of two-step HRE. Dynamic recrystallization and adjacent grain broking during HRE is introduced to explain the effects of one-step and two-step HRE on the microstructure and mechanical properties of AZ31 Mg alloy. The current results imply that the simple HRE method might be a feasible processing method for industry applications, and the multiply steps extrusion are effective to fabricate high strength of fine grained hcp metals.
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