The structures of (q5-C5Me5),Zr(0H)(CI) (1) and ( T ~-C ~M ~~) ~Z ~( O H ) ~(2) have been determined by X-ray diffraction; location of all hydrogen atoms in (1) has established the presence of significant intramolecular non-bonding contacts and (2) is the first early transition metal dihydroxo complex to be structurally characterized.
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