The following list comprises results obtained during 1970 from both the 1 L and 6 L counters. Results are not corrected for C13fractionation. Errors quoted refer only to the standard deviation calculated from a statistical analysis of sample and background count rates and the Libby half-life of 5570 ± 30 yr. Pretreatment has been continued as described previously (R., 1969, v. 11, p. 263). In cases where sample size was insufficient for full pretreatment, details of the necessary deviations accompany the result.
The following list of dates contains all measurements made during 1972, i.e., since our last list. Counting equipment, operating procedures and sample pretreatment are the same as previously described (R., 1969, v. 11, p. 263). Age calculations are based on 95% activity of the NBS oxalic acid standard computed from the Libby half-life of 5570 ± 30 yr. Background samples are synthesized from Welsh anthracite. Errors quoted refer only to the standard deviation (1σ) calculated from a statistical analysis of sample, background and standard count rates.
Measurements have continued with the 6 L counter which has proved reliable at pressures as high as 2.6 atm and as low as 0.3 atm. It has now been enclosed in a double ring of 27 geiger tubes which has reduced the background count to 10 cpm at 2 atm. So far, we have had no success with the 1.5 L Oeschger-type proportional counter. Failure to obtain steady readings is probably due to continued outgassing from the teflon insulation. All insulating parts have now been remanufactured from the same source of teflon as was used in the 6 L counter, and the Oeschger counter is being reassembled.Results are still given without correction for δC13. Errors quoted refer only to the standard deviation calculated from a statistical analysis of count rates and the Libby half-life of 5570 ± 30 yr.
Measurements have continued with both the 1 L and 6 L counters. Results are not corrected for C13 fractionation. Errors quoted refer only to the standard deviation calculated from a statistical analysis of sample and background count rates and the Libby half-life of 5570 ± 30 yr. Pretreatment has been continued as described previously (Shotton, Blundell, and Williams, 1969).
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