Photochemical vapor generation of Os. OsO4 oxidative product from photolysis of 5% HNO3 medium; reductive product from 1% acetic acid/50 mg L−1 Fe3/2+ an uncharacterized organometallic Os compound [Osw(CO)x(CH3)yHz] detected by ICP-MS.
The results originated from the application of a simple and straightforward photochemical reactor to generate volatile species from noble metals (Au, Ir, Pd, Pt and Rh) are presented.
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