a) File of Results for CS Aliquots from Rod B and (b) File of Results for ZR Aliquots from Rod B 27. Data File Containing Results of Mass Spectrometric Measurements to Determine Plenum-Gas Compositions 28. Data File Containing Results of Mass Spectrometric Measurements to Determine Xe and Kr Isotopy in Plenum-Gas Samples 29. Data File Containing Results of Mass Spectrometric Measurements to Determine Dissolver Off-gas Composition 140 30. Selected Frames from High-Speed Motion Pictures of the Shearing Process 149 31. Correlation Between Fission Gas and 137 Cs in Rod Segments 185 B-l. Difference Between 232 U/ 233 U Isotope Ratios as Measured by Mass Spectrometry and Alpha Counting as a Function of the Alpha-Counting Ratio 206 D-l. Deviations from Average for Duplicate Determinations of U3T Uranium Concentration for LWBR Fuel Rod Segments 228 D-2. Deviations from Average for 233 U/ 238 U Ratios Determined Using Duplicate Samples of Spiked Blend Tank Solution 234 D-3. Deviations Between 950a-MSID and 993-MSID Uranium Assay Results for LWBR Fuel Rod Segments 234 LIST OF TABLES No. Ease 1. Limits to Allowable Error in Fuel Rod Parameters: DOE-NR Error Requirements 15 2. Limits to Allowable Error in ANL Measurements and Analyses: Project Error Requirements 17 3. Nominal Characteristics of the Four Types of LWBR Fuel Rods Processed at ANL 19 4. Source and Analysis Codes for EOL Samples 60 5. Fuel Rod Shipments Received at ANL during the EOL Campaign 64 6. Dissolver 2 Process Control States 88 7. Results of Measurements from Calibration of 234 U/ 236 U Internal Standard 119 8. Abundances of Minor Isotopes in "^U/ 236 !! Internal Standard 9. Types of Analysis Available for Execution by the Automated Gamma-Counting Programs 10. Half-Lives of Selected Fission Products and Factors for Converting Microcurie Units to Atoms 11. Weights of LWBR Fuel Rods Measured Before and After Puncture of the Fuel Rod Plenum Region 12. Results of Post-EOL Test to Check Shear Feed System Performance 146 13. Deviations Between As-Cut Locations of Segment Boundaries and Specified Locations for LWBR Fuel Rods 150 14. Approximate Fuel Recovery for Rods Processed in the EOL Campaign 157 15. Extent of Dissolution in the Primary Dissolution for LWBR Fuel Rod Segments 159 16. Results of Blank Dissolution Runs Following Fuel Rod Dissolutions 161 17. Radiation Levels Measured for Filters Used in Dissolution of Fuel Rod Segments 163 via LIST OF TABLES (contd) No. Page 18. Fission Products Found on Filter from Dissolution of Segment B-04 164 19. Contributions to Uncertainty in Measured Weight of Solution Removed from the Dissolver System As Samples 20. Summary of Estimated Fractional Fuel Losses During Dissolver Operations 21. Estimates of Maximum Probable Bias in Weight Percent Abundances Reported for Individual Uranium Isotopes 22. Data from Individual Analyses of UNH Reference Material 23. Summary of Uranium and Thorium Assay Results for Dissolved Plenum Segments 178 24. Sums of Segment Uranium Assay Results and Estimated Limits to Probable Error for L...

Photochlorination of 2-Chloro-2-methylpropanb 1027 for the length of time given in Column 4, Table II, before earbonation. It was usually necessary to warm the mixture at the start in order to initiate the reaction. Conditions and yields are summarized in Table II. ConclusionsWhen diamyl mercury was treated with sodium and the product of the reaction carbonated, yields as high as 40-50% of butylmalonic acid were obtained. Diethyl mercury by the same Oak Park, Illinois

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