An experimental study was carried out to evaluate the effect of several fibers on the mechanical properties, drying shrinkage, and microstructural characteristics of alkali‐activated kaolin binders. Four different types of fibers were evaluated in this study: polypropylene (PP) fiber, discontinuous structural synthetic (DSS) fiber, brass‐coated steel (BCS) fiber, and hooked steel (HS) fiber. The fibers were added to the alkali‐activated kaolin at a volume fraction of 0%, 0.5%, 1%, and 1.5%. The experimental results revealed that the compressive strength of alkali‐activated binder increased by about 60% when 1% of PP fiber is added, whereas the addition of HS fiber substantially enhanced the flexural strength (more than 200% when 1.5% fiber volume content is added). BCS and HS fibers were found to more effective compared to PP and DSS fibers in maintaining the binder integrity prior to high temperatures exposure. All fiber‐reinforced alkali‐activated composites yielded lower drying shrinkage (≤450 microstrains), where HS fiber was found to effectively prevent the shrinkage of the binder (≤60 microstrains). The microstructural investigation revealed good interfacial bonding between the alkali‐activated binder and the fibers.

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